9-Benzyl-3-methyladenine Perchlorate

Base Information

• Chemical Name: 9-Benzyl-3-methyladenine Perchlorate
• CAS No.: 70276-37-8
• Molecular Formula: C₁₃H₁₃N₅*ClHO₄
• Molecular Weight: 339.738
• Mol file: 70276-37-8.mol

Synonyms:9-Benzyl-3-methyladenine Perchlorate

Chemical Property of 9-Benzyl-3-methyladenine Perchlorate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-Benzyl-3-methyladenine Perchlorate

There total 6 articles about 9-Benzyl-3-methyladenine Perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

9-Benzyl-N6-ethoxy-3-methyladenine Perchlorate (125661-70-3) → 9-Benzyl-3-methyladenine Perchlorate (70276-37-8)

Guidance literature:

With hydrogen; Raney Ni W-2; In methanol; for 24h; under 760 Torr; Ambient temperature;

DOI:10.1248/cpb.37.1504

Reference yield:

1-Benzyl-N'-ethoxy-5-(methylamino)-1H-imidazole-4-carboxamidine Dihydrochloride (125661-65-6) → 9-Benzyl-3-methyladenine Perchlorate (70276-37-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.) NaClO₄*H₂O / 1.) MeOH, room temperature, 2 h, 2.) water,

2: 34 percent / H₂ / Raney Ni W-2 / methanol / 24 h / 760 Torr / Ambient temperature

With sodium perchlorate; hydrogen; Raney Ni W-2; In methanol;

DOI:10.1248/cpb.37.1504

Reference yield:

1-Benzyl-N'-ethoxy-5-formamido-1H-imidazole-4-carboxamidine (70276-43-6,125661-60-1,125661-61-2) → 9-Benzyl-3-methyladenine Perchlorate (70276-37-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / anhydrous K₂CO₃ / dimethylformamide / 3 h / Ambient temperature

2: 1.) H₂, 1N aqueous HCl,2.) Et₃N, 70percent aqueous HClO₄ / 1.) room temperature, 3 h, 2.) EtOH, 80 deg C,

With hydrogenchloride; perchloric acid; hydrogen; potassium carbonate; triethylamine; In N,N-dimethyl-formamide;

DOI:10.1248/cpb.37.1504

upstream raw materials:

9-Benzyl-N⁶-ethoxy-3-methyladenine Perchlorate

1-benzyl-5-(N-methylformamido)-1H-imidazole-4-carboxamidine perchlorate

1-Benzyl-N'-ethoxy-5-(N-methylformamido)-1H-imidazole-4-carboxamidine

1-Benzyl-N'-ethoxy-5-formamido-1H-imidazole-4-carboxamidine

Downstream raw materials:

1-benzyl-5-(N-methylformamido)-1H-imidazole-4-carboxamidine perchlorate