Technology Process of 5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone
There total 4 articles about 5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium cerium(IV) nitrate; acetic acid;
In
water; acetonitrile;
at 50 ℃;
for 0.5h;
DOI:10.1021/jo0494681
- Guidance literature:
-
Multi-step reaction with 3 steps
1: H2 / Pd(OH)2/C / methanol; ethyl acetate / 1.5 h / 20 °C / 760 Torr
2: 4-dimethylaminopyridine; pyridine / 1 h / 60 °C
3: 43 percent / ceric ammonium nitrite; acetic acid / acetonitrile; H2O / 0.5 h / 50 °C
With
pyridine; dmap; ammonium cerium(IV) nitrate; hydrogen; acetic acid;
palladium dihydroxide;
In
methanol; water; ethyl acetate; acetonitrile;
DOI:10.1021/jo0494681
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 4-dimethylaminopyridine; pyridine / 1 h / 60 °C
2: 43 percent / ceric ammonium nitrite; acetic acid / acetonitrile; H2O / 0.5 h / 50 °C
With
pyridine; dmap; ammonium cerium(IV) nitrate; acetic acid;
In
water; acetonitrile;
DOI:10.1021/jo0494681
