5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone

Base Information

Chemical Name:5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone
CAS No.:749256-78-8
Molecular Formula:C₅₄H₄₄O₁₆
Molecular Weight:948.934
Hs Code.:

Synonyms:5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone

Suppliers and Price of 5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone

There total 4 articles about 5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 749256-77-7
5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavan

: 749256-78-8
5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone

Guidance literature:: With ammonium cerium(IV) nitrate; acetic acid; In water; acetonitrile; at 50 ℃; for 0.5h;
DOI:10.1021/jo0494681

Reference yield:

: 749256-76-6
5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-methoxyflavan

: 749256-78-8
5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd(OH)2/C / methanol; ethyl acetate / 1.5 h / 20 °C / 760 Torr

2: 4-dimethylaminopyridine; pyridine / 1 h / 60 °C

3: 43 percent / ceric ammonium nitrite; acetic acid / acetonitrile; H₂O / 0.5 h / 50 °C

With pyridine; dmap; ammonium cerium(IV) nitrate; hydrogen; acetic acid; palladium dihydroxide; In methanol; water; ethyl acetate; acetonitrile;
DOI:10.1021/jo0494681

Reference yield:

: 98-88-4
benzoyl chloride

: 749256-78-8
5,4'-diacetoxy-6-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-7-methoxyflavanone

Guidance literature:: Multi-step reaction with 2 steps

1: 4-dimethylaminopyridine; pyridine / 1 h / 60 °C

2: 43 percent / ceric ammonium nitrite; acetic acid / acetonitrile; H₂O / 0.5 h / 50 °C

With pyridine; dmap; ammonium cerium(IV) nitrate; acetic acid; In water; acetonitrile;
DOI:10.1021/jo0494681