4-tert-butyl-2-(5-tert-butyl-2-hydroxyphenylsulfanyl)-6-(hydroxymethyl)phenol

Base Information

Chemical Name:4-tert-butyl-2-(5-tert-butyl-2-hydroxyphenylsulfanyl)-6-(hydroxymethyl)phenol
CAS No.:133786-62-6
Molecular Formula:C₂₁H₂₈O₃S
Molecular Weight:360.518
Hs Code.:

Synonyms:4-tert-butyl-2-(5-tert-butyl-2-hydroxyphenylsulfanyl)-6-(hydroxymethyl)phenol

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Chemical Property of 4-tert-butyl-2-(5-tert-butyl-2-hydroxyphenylsulfanyl)-6-(hydroxymethyl)phenol

Chemical Property:

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Technology Process of 4-tert-butyl-2-(5-tert-butyl-2-hydroxyphenylsulfanyl)-6-(hydroxymethyl)phenol

There total 3 articles about 4-tert-butyl-2-(5-tert-butyl-2-hydroxyphenylsulfanyl)-6-(hydroxymethyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 3273-24-3
2,2'-thiobis<4-t-butylphenol>

: 133786-62-6
4-tert-butyl-2-(5-tert-butyl-2-hydroxyphenylsulfanyl)-6-(hydroxymethyl)phenol

Guidance literature:: With sodium hydroxide; In water; at 50 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c5cc00819k

Reference yield: 33.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 3273-24-3
2,2'-thiobis<4-t-butylphenol>

: 133786-62-6
4-tert-butyl-2-(5-tert-butyl-2-hydroxyphenylsulfanyl)-6-(hydroxymethyl)phenol

: 133786-63-7
4,4'-di(tert-butyl)-2,2'-bis(hydroxymethyl)-6,6'-sulfandiyldiphenol

Guidance literature:: With sodium hydroxide; In methanol; water; at 50 ℃; for 26h;
DOI:10.1246/bcsj.64.576

Reference yield:

: 98-54-4
para-tert-butylphenol

: 133786-62-6
4-tert-butyl-2-(5-tert-butyl-2-hydroxyphenylsulfanyl)-6-(hydroxymethyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / SCl₂ / CH₂Cl₂ / 1 h / 0 °C

2: 47 percent / 10percent NaOH / methanol; H₂O / 26 h / 50 °C

With sodium hydroxide; sulfur dichloride; In methanol; dichloromethane; water;
DOI:10.1246/bcsj.64.576