malonic acid 2,6-di-tert-butyl-4-[4-[3,5-di-tert-butyl-4-(3-hydroxy-propoxy)-phenylsulfanyl]-1-(2-methoxycarbonyl-acetyl)-piperidin-4-ylsulfanyl]-phenyl ester methyl ester

Base Information

Chemical Name:malonic acid 2,6-di-tert-butyl-4-[4-[3,5-di-tert-butyl-4-(3-hydroxy-propoxy)-phenylsulfanyl]-1-(2-methoxycarbonyl-acetyl)-piperidin-4-ylsulfanyl]-phenyl ester methyl ester
CAS No.:1402049-75-5
Molecular Formula:C₄₄H₆₅NO₉S₂
Molecular Weight:816.133
Hs Code.:

malonic acid 2,6-di-tert-butyl-4-[4-[3,5-di-tert-butyl-4-(3-hydroxy-propoxy)-phenylsulfanyl]-1-(2-methoxycarbonyl-acetyl)-piperidin-4-ylsulfanyl]-phenyl ester methyl ester

Synonyms:malonic acid 2,6-di-tert-butyl-4-[4-[3,5-di-tert-butyl-4-(3-hydroxy-propoxy)-phenylsulfanyl]-1-(2-methoxycarbonyl-acetyl)-piperidin-4-ylsulfanyl]-phenyl ester methyl ester

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Chemical Property of malonic acid 2,6-di-tert-butyl-4-[4-[3,5-di-tert-butyl-4-(3-hydroxy-propoxy)-phenylsulfanyl]-1-(2-methoxycarbonyl-acetyl)-piperidin-4-ylsulfanyl]-phenyl ester methyl ester

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Technology Process of malonic acid 2,6-di-tert-butyl-4-[4-[3,5-di-tert-butyl-4-(3-hydroxy-propoxy)-phenylsulfanyl]-1-(2-methoxycarbonyl-acetyl)-piperidin-4-ylsulfanyl]-phenyl ester methyl ester

There total 3 articles about malonic acid 2,6-di-tert-butyl-4-[4-[3,5-di-tert-butyl-4-(3-hydroxy-propoxy)-phenylsulfanyl]-1-(2-methoxycarbonyl-acetyl)-piperidin-4-ylsulfanyl]-phenyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 37517-81-0
3-chloro-3-oxopropanoic acid methyl ester

: 1402047-98-6
2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(3-hydroxypropoxy)phenylsulfanyl]-piperidin-4-ylsulfanyl}phenol

: 1402049-75-5
malonic acid 2,6-di-tert-butyl-4-[4-[3,5-di-tert-butyl-4-(3-hydroxy-propoxy)-phenylsulfanyl]-1-(2-methoxycarbonyl-acetyl)-piperidin-4-ylsulfanyl]-phenyl ester methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield:

: 1402049-10-8
4,4-bis-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)piperidine-1-carboxylic acid ethyl ester

: 1402049-75-5
malonic acid 2,6-di-tert-butyl-4-[4-[3,5-di-tert-butyl-4-(3-hydroxy-propoxy)-phenylsulfanyl]-1-(2-methoxycarbonyl-acetyl)-piperidin-4-ylsulfanyl]-phenyl ester methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 85 °C

2: sodium hydroxide; 2-methoxy-ethanol / 18 h / 120 °C

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C

With 2-methoxy-ethanol; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 950-59-4
4-hydroxy-3,5-di-tert-butylthiophenol

: 1402049-75-5
malonic acid 2,6-di-tert-butyl-4-[4-[3,5-di-tert-butyl-4-(3-hydroxy-propoxy)-phenylsulfanyl]-1-(2-methoxycarbonyl-acetyl)-piperidin-4-ylsulfanyl]-phenyl ester methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / methanol / 20 h / 45 °C

2: potassium carbonate / N,N-dimethyl-formamide / 6 h / 85 °C

3: sodium hydroxide; 2-methoxy-ethanol / 18 h / 120 °C

4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C

With hydrogenchloride; 2-methoxy-ethanol; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;