di-(p-nitrobenzyl) azodicarboxylate

Base Information

Chemical Name:di-(p-nitrobenzyl) azodicarboxylate
CAS No.:1191377-56-6
Molecular Formula:C₁₆H₁₂N₄O₈
Molecular Weight:388.293
Hs Code.:

Synonyms:di-(p-nitrobenzyl) azodicarboxylate

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Chemical Property of di-(p-nitrobenzyl) azodicarboxylate

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Technology Process of di-(p-nitrobenzyl) azodicarboxylate

There total 2 articles about di-(p-nitrobenzyl) azodicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 157984-22-0
di-p-nitrobenzyl hydrazine-1,2-dicarboxylate

: 1191377-56-6
di-(p-nitrobenzyl) azodicarboxylate

Guidance literature:: With pyridine; bromine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.12.036

Reference yield:

: 4457-32-3
4-nitrobenzyl chloroformate

: 1191377-56-6
di-(p-nitrobenzyl) azodicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; hydrazine hydrate / water; toluene / 6 h / 20 °C

2: pyridine; bromine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; bromine; sodium hydrogencarbonate; hydrazine hydrate; In dichloromethane; water; toluene;
DOI:10.1016/j.tet.2010.12.036