4-chloro-1-{[6-ethoxy-1-(2-methylpropyl)benzimidazole-2-yl]methoxy}benzene

Base Information

Chemical Name:4-chloro-1-{[6-ethoxy-1-(2-methylpropyl)benzimidazole-2-yl]methoxy}benzene
CAS No.:1446337-69-4
Molecular Formula:C₂₀H₂₃ClN₂O₂
Molecular Weight:358.868
Hs Code.:

Synonyms:4-chloro-1-{[6-ethoxy-1-(2-methylpropyl)benzimidazole-2-yl]methoxy}benzene

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Chemical Property of 4-chloro-1-{[6-ethoxy-1-(2-methylpropyl)benzimidazole-2-yl]methoxy}benzene

Chemical Property:

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Technology Process of 4-chloro-1-{[6-ethoxy-1-(2-methylpropyl)benzimidazole-2-yl]methoxy}benzene

There total 6 articles about 4-chloro-1-{[6-ethoxy-1-(2-methylpropyl)benzimidazole-2-yl]methoxy}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1446338-18-6
2-(4-chlorophenoxy)-N-{4-ethoxy-2-[(2-methylpropyl)amino]phenyl}acetamide

: 1446337-69-4
4-chloro-1-{[6-ethoxy-1-(2-methylpropyl)benzimidazole-2-yl]methoxy}benzene

Guidance literature:: With acetic acid; at 100 ℃; for 1h;

Reference yield:

: 122-88-3
4-Chlorophenoxyacetic acid

: 1446337-69-4
4-chloro-1-{[6-ethoxy-1-(2-methylpropyl)benzimidazole-2-yl]methoxy}benzene

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane

2: potassium carbonate / acetonitrile / 3.75 h / 20 °C / Inert atmosphere

3: acetic acid / 1 h / 100 °C

With oxalyl dichloride; potassium carbonate; acetic acid; N,N-dimethyl-formamide; In dichloromethane; acetonitrile;

Reference yield:

: 28987-48-6
4-ethoxy-2-fluoro-1-nitrobenzene

: 1446337-69-4
4-chloro-1-{[6-ethoxy-1-(2-methylpropyl)benzimidazole-2-yl]methoxy}benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 1 h / 100 °C / Sealed tube

2: palladium 10% on activated carbon; hydrogen / ethanol

3: potassium carbonate / acetonitrile / 3.75 h / 20 °C / Inert atmosphere

4: acetic acid / 1 h / 100 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; acetic acid; In ethanol; acetonitrile;