N¹-(4-((2-adamantylacetamido)methyl)phenyl)-N¹-methyl-N²-methyl-N²-methyloxyoxalamide

Base Information

• Chemical Name: N¹-(4-((2-adamantylacetamido)methyl)phenyl)-N¹-methyl-N²-methyl-N²-methyloxyoxalamide
• CAS No.: 1542915-50-3
• Molecular Formula: C₂₄H₃₃N₃O₄
• Molecular Weight: 427.544

Synonyms:N¹-(4-((2-adamantylacetamido)methyl)phenyl)-N¹-methyl-N²-methyl-N²-methyloxyoxalamide

Chemical Property of N¹-(4-((2-adamantylacetamido)methyl)phenyl)-N¹-methyl-N²-methyl-N²-methyloxyoxalamide

Chemical Property:

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Technology Process of N¹-(4-((2-adamantylacetamido)methyl)phenyl)-N¹-methyl-N²-methyl-N²-methyloxyoxalamide

There total 5 articles about N¹-(4-((2-adamantylacetamido)methyl)phenyl)-N¹-methyl-N²-methyl-N²-methyloxyoxalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-aminomethyl)aniline (4403-71-8) → N1-(4-((2-adamantylacetamido)methyl)phenyl)-N1-methyl-N2-methyl-N2-methyloxyoxalamide (1542915-50-3)

Guidance literature:

Multi-step reaction with 5 steps

1.1: dmap / dichloromethane / 0.17 h / 20 °C

1.2: 20 °C

2.1: triethylamine / dichloromethane / 0 - 20 °C

3.1: water; sodium hydroxide / ethanol / 20 °C

4.1: dmap; triethylamine / dichloromethane / 0.17 h / 20 °C

4.2: 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With dmap; water; potassium carbonate; triethylamine; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2013.12.027

Reference yield:

N1-(4-((2-adamantylacetamido)methyl)phenyl)-N2-methyl-N2-methyloxyoxalamide + methyl iodide (74-88-4) → N1-(4-((2-adamantylacetamido)methyl)phenyl)-N1-methyl-N2-methyl-N2-methyloxyoxalamide (1542915-50-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.bmc.2013.12.027

Reference yield:

C19H26N2O (1542915-79-6) → N1-(4-((2-adamantylacetamido)methyl)phenyl)-N1-methyl-N2-methyl-N2-methyloxyoxalamide (1542915-50-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C

2.1: water; sodium hydroxide / ethanol / 20 °C

3.1: dmap; triethylamine / dichloromethane / 0.17 h / 20 °C

3.2: 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With dmap; water; potassium carbonate; triethylamine; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2013.12.027

upstream raw materials:

C₁₉H₂₆N₂O

C₂₃H₃₀N₂O₄

methyl iodide

(4-aminomethyl)aniline

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