Technology Process of C57H70N4O10
There total 15 articles about C57H70N4O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: 95 percent / NaOH / tetrahydrofuran / 3 h / 20 °C
2.1: triethylamine; tert-butyl hypochlorite / tetrahydrofuran / 0.33 h
2.2: ZnCl2 / tetrahydrofuran / 0.08 h
2.3: 89 percent / tetrahydrofuran / -60 - 20 °C
3.1: 96 percent / HCl / methanol / 2 h / 40 °C
4.1: 71 percent / toluene / 5 h / Heating
5.1: 76 percent / Lawesson's reagent / toluene / 12 h / Heating
6.1: NaBH4 / NiCl2
7.1: 96 percent / toluene / 12 h / Heating
8.1: triethylamine; tert-butyl hypochlorite / CH2Cl2 / 0.08 h / 0 °C
9.1: tetrafluoroboric acid-diethyl ether complex; silver tetrafluoroborate / acetone / 0.08 h
With
Lawessons reagent; hydrogenchloride; tetrafluoroboric acid diethyl ether; sodium hydroxide; sodium tetrahydroborate; silver tetrafluoroborate; tert-butylhypochlorite; triethylamine;
nickel dichloride;
In
tetrahydrofuran; methanol; dichloromethane; acetone; toluene;
DOI:10.1021/jo000249z
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: sodium borohydride / methanol / 0.42 h / 0 °C
2.1: 95 percent / NaOH / tetrahydrofuran / 3 h / 20 °C
3.1: triethylamine; tert-butyl hypochlorite / tetrahydrofuran / 0.33 h
3.2: ZnCl2 / tetrahydrofuran / 0.08 h
3.3: 89 percent / tetrahydrofuran / -60 - 20 °C
4.1: 96 percent / HCl / methanol / 2 h / 40 °C
5.1: 71 percent / toluene / 5 h / Heating
6.1: 76 percent / Lawesson's reagent / toluene / 12 h / Heating
7.1: NaBH4 / NiCl2
8.1: 96 percent / toluene / 12 h / Heating
9.1: triethylamine; tert-butyl hypochlorite / CH2Cl2 / 0.08 h / 0 °C
10.1: tetrafluoroboric acid-diethyl ether complex; silver tetrafluoroborate / acetone / 0.08 h
With
Lawessons reagent; hydrogenchloride; tetrafluoroboric acid diethyl ether; sodium hydroxide; sodium tetrahydroborate; silver tetrafluoroborate; tert-butylhypochlorite; triethylamine;
nickel dichloride;
In
tetrahydrofuran; methanol; dichloromethane; acetone; toluene;
DOI:10.1021/jo000249z
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: triethylamine; tert-butyl hypochlorite / tetrahydrofuran / 0.33 h
1.2: ZnCl2 / tetrahydrofuran / 0.08 h
1.3: 89 percent / tetrahydrofuran / -60 - 20 °C
2.1: 96 percent / HCl / methanol / 2 h / 40 °C
3.1: 71 percent / toluene / 5 h / Heating
4.1: 76 percent / Lawesson's reagent / toluene / 12 h / Heating
5.1: NaBH4 / NiCl2
6.1: 96 percent / toluene / 12 h / Heating
7.1: triethylamine; tert-butyl hypochlorite / CH2Cl2 / 0.08 h / 0 °C
8.1: tetrafluoroboric acid-diethyl ether complex; silver tetrafluoroborate / acetone / 0.08 h
With
Lawessons reagent; hydrogenchloride; tetrafluoroboric acid diethyl ether; sodium tetrahydroborate; silver tetrafluoroborate; tert-butylhypochlorite; triethylamine;
nickel dichloride;
In
tetrahydrofuran; methanol; dichloromethane; acetone; toluene;
DOI:10.1021/jo000249z
