5-(4-chlorophenyl)-4-methyl-1-[4-(trifluoromethyl)phenyl]-N-(piperidin-1-yl)-1H-pyrazole-3-carboxamide

Base Information

Chemical Name:5-(4-chlorophenyl)-4-methyl-1-[4-(trifluoromethyl)phenyl]-N-(piperidin-1-yl)-1H-pyrazole-3-carboxamide
CAS No.:1291068-00-2
Molecular Formula:C₂₃H₂₂ClF₃N₄O
Molecular Weight:462.902
Hs Code.:

Synonyms:5-(4-chlorophenyl)-4-methyl-1-[4-(trifluoromethyl)phenyl]-N-(piperidin-1-yl)-1H-pyrazole-3-carboxamide

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Chemical Property of 5-(4-chlorophenyl)-4-methyl-1-[4-(trifluoromethyl)phenyl]-N-(piperidin-1-yl)-1H-pyrazole-3-carboxamide

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Technology Process of 5-(4-chlorophenyl)-4-methyl-1-[4-(trifluoromethyl)phenyl]-N-(piperidin-1-yl)-1H-pyrazole-3-carboxamide

There total 9 articles about 5-(4-chlorophenyl)-4-methyl-1-[4-(trifluoromethyl)phenyl]-N-(piperidin-1-yl)-1H-pyrazole-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1291068-17-1
C₁₈H₁₁Cl₂F₃N₂O

: 2213-43-6
1-Aminopiperidine

: 1291068-00-2
5-(4-chlorophenyl)-4-methyl-1-[4-(trifluoromethyl)phenyl]-N-(piperidin-1-yl)-1H-pyrazole-3-carboxamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.3109/14756366.2010.491794

Reference yield:

: 1291068-13-7
C₂₀H₁₆ClF₃N₂O₂

: 1291068-00-2
5-(4-chlorophenyl)-4-methyl-1-[4-(trifluoromethyl)phenyl]-N-(piperidin-1-yl)-1H-pyrazole-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: water; potassium hydroxide / ethanol / 3 h / Reflux

2: thionyl chloride / toluene / 3 h / Reflux

3: triethylamine / dichloromethane / 0 - 20 °C

With thionyl chloride; water; triethylamine; potassium hydroxide; In ethanol; dichloromethane; toluene;
DOI:10.3109/14756366.2010.491794

Reference yield:

: 1291068-15-9
5-(4-chlorophenyl)-4-methyl-1-[4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carboxylic acid

: 1291068-00-2
5-(4-chlorophenyl)-4-methyl-1-[4-(trifluoromethyl)phenyl]-N-(piperidin-1-yl)-1H-pyrazole-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / toluene / 3 h / Reflux

2: triethylamine / dichloromethane / 0 - 20 °C

With thionyl chloride; triethylamine; In dichloromethane; toluene;
DOI:10.3109/14756366.2010.491794