ethyl 2-{2-iso-propyl-4-[(4-methyl-2-(4-trifluoromethylphenyl)thiazol-5-yl)methylthio]phenoxy}acetate

Base Information

Chemical Name:ethyl 2-{2-iso-propyl-4-[(4-methyl-2-(4-trifluoromethylphenyl)thiazol-5-yl)methylthio]phenoxy}acetate
CAS No.:1268500-94-2
Molecular Formula:C₂₅H₂₆F₃NO₃S₂
Molecular Weight:509.614
Hs Code.:

Synonyms:ethyl 2-{2-iso-propyl-4-[(4-methyl-2-(4-trifluoromethylphenyl)thiazol-5-yl)methylthio]phenoxy}acetate

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Chemical Property of ethyl 2-{2-iso-propyl-4-[(4-methyl-2-(4-trifluoromethylphenyl)thiazol-5-yl)methylthio]phenoxy}acetate

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Technology Process of ethyl 2-{2-iso-propyl-4-[(4-methyl-2-(4-trifluoromethylphenyl)thiazol-5-yl)methylthio]phenoxy}acetate

There total 4 articles about ethyl 2-{2-iso-propyl-4-[(4-methyl-2-(4-trifluoromethylphenyl)thiazol-5-yl)methylthio]phenoxy}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1268500-82-8
2-iso-propyl-4-{[4-methyl-2-(4-trifluoromethylphenyl)thiazol-5-yl]methylthio}phenol

: 105-36-2
ethyl bromoacetate

: 1268500-94-2
ethyl 2-{2-iso-propyl-4-[(4-methyl-2-(4-trifluoromethylphenyl)thiazol-5-yl)methylthio]phenoxy}acetate

Guidance literature:: With caesium carbonate; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1002/ardp.201000189

Reference yield:

: 1268500-77-1
2-iso-propyl-4-mercaptophenol

: 1268500-94-2
ethyl 2-{2-iso-propyl-4-[(4-methyl-2-(4-trifluoromethylphenyl)thiazol-5-yl)methylthio]phenoxy}acetate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / acetonitrile / 4 h / 20 °C / Inert atmosphere

2: caesium carbonate / acetonitrile / 20 °C / Inert atmosphere

With caesium carbonate; In acetonitrile;
DOI:10.1002/ardp.201000189

Reference yield:

: 88-69-7
2-(1-methylethyl)phenol

: 1268500-94-2
ethyl 2-{2-iso-propyl-4-[(4-methyl-2-(4-trifluoromethylphenyl)thiazol-5-yl)methylthio]phenoxy}acetate

Guidance literature:: Multi-step reaction with 4 steps

1: bromine; sodium bromide / methanol / 3 h / 0 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: caesium carbonate / acetonitrile / 4 h / 20 °C / Inert atmosphere

4: caesium carbonate / acetonitrile / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; bromine; caesium carbonate; sodium bromide; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1002/ardp.201000189