1-((2-(3-(cyclopenta-2,4-dienylidene)propoxy)ethoxy)methyl)-4-methoxybenzene

Base Information

Chemical Name:1-((2-(3-(cyclopenta-2,4-dienylidene)propoxy)ethoxy)methyl)-4-methoxybenzene
CAS No.:1351600-77-5
Molecular Formula:C₁₈H₂₂O₃
Molecular Weight:286.371
Hs Code.:

Synonyms:1-((2-(3-(cyclopenta-2,4-dienylidene)propoxy)ethoxy)methyl)-4-methoxybenzene

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Chemical Property of 1-((2-(3-(cyclopenta-2,4-dienylidene)propoxy)ethoxy)methyl)-4-methoxybenzene

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Technology Process of 1-((2-(3-(cyclopenta-2,4-dienylidene)propoxy)ethoxy)methyl)-4-methoxybenzene

There total 3 articles about 1-((2-(3-(cyclopenta-2,4-dienylidene)propoxy)ethoxy)methyl)-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13807-89-1
2-(4-methoxybenzyloxy)ethanol

: 1351600-77-5
1-((2-(3-(cyclopenta-2,4-dienylidene)propoxy)ethoxy)methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

1.2: 12 h / 0 - 20 °C / Inert atmosphere

2.1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.2: 12 h / 20 °C / Inert atmosphere

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 20 °C / Inert atmosphere

4.1: pyrrolidine / methanol / 2 h / 20 °C / Inert atmosphere

With pyrrolidine; dimethylsulfide borane complex; sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja108516b

Reference yield:

: 1351600-76-4
3-(2-(4-methoxybenzyloxy)ethoxy)propan-1-ol

: 1351600-77-5
1-((2-(3-(cyclopenta-2,4-dienylidene)propoxy)ethoxy)methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 20 °C / Inert atmosphere

2: pyrrolidine / methanol / 2 h / 20 °C / Inert atmosphere

With pyrrolidine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; dimethyl sulfoxide;
DOI:10.1021/ja108516b

Reference yield:

: 1351600-75-3
1-((2-(allyloxy)ethoxy)methyl)-4-methoxybenzene

: 1351600-77-5
1-((2-(3-(cyclopenta-2,4-dienylidene)propoxy)ethoxy)methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 20 °C / Inert atmosphere

3.1: pyrrolidine / methanol / 2 h / 20 °C / Inert atmosphere

With pyrrolidine; dimethylsulfide borane complex; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dimethyl sulfoxide;
DOI:10.1021/ja108516b