(5S,6R)-2,2'-anhydro-1-(3'-bromo-3'-deoxy-5'-O-trityl-β-D-arabinofuranosyl)-5,6-epoxy-5,6-dihydrothymine

Base Information

Chemical Name:(5S,6R)-2,2'-anhydro-1-(3'-bromo-3'-deoxy-5'-O-trityl-β-D-arabinofuranosyl)-5,6-epoxy-5,6-dihydrothymine
CAS No.:145819-52-9
Molecular Formula:C₂₉H₂₅BrN₂O₅
Molecular Weight:561.432
Hs Code.:

Synonyms:(5S,6R)-2,2'-anhydro-1-(3'-bromo-3'-deoxy-5'-O-trityl-β-D-arabinofuranosyl)-5,6-epoxy-5,6-dihydrothymine

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Chemical Property of (5S,6R)-2,2'-anhydro-1-(3'-bromo-3'-deoxy-5'-O-trityl-β-D-arabinofuranosyl)-5,6-epoxy-5,6-dihydrothymine

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Technology Process of (5S,6R)-2,2'-anhydro-1-(3'-bromo-3'-deoxy-5'-O-trityl-β-D-arabinofuranosyl)-5,6-epoxy-5,6-dihydrothymine

There total 1 articles about (5S,6R)-2,2'-anhydro-1-(3'-bromo-3'-deoxy-5'-O-trityl-β-D-arabinofuranosyl)-5,6-epoxy-5,6-dihydrothymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 145819-51-8
2,2'-anhydro-1-(3'-deoxy-3'-bromo-5'-O-trityl-β-D-arabinofuranosyl)-(5R,6R)-trans-5-bromo-6-hydroxy-5,6-dihydrothymine

: 145819-52-9
(5S,6R)-2,2'-anhydro-1-(3'-bromo-3'-deoxy-5'-O-trityl-β-D-arabinofuranosyl)-5,6-epoxy-5,6-dihydrothymine

Guidance literature:: With triethylamine; In acetone; for 5h; Heating;
DOI:10.1246/cl.1992.2149

Reference yield: 48.0%

: 145819-52-9
(5S,6R)-2,2'-anhydro-1-(3'-bromo-3'-deoxy-5'-O-trityl-β-D-arabinofuranosyl)-5,6-epoxy-5,6-dihydrothymine

: 145819-53-0
2,2'-anhydro-1-(3'-deoxy-3'-bromo-5'-O-trityl-β-D-arabinofuranosyl)thymine

Guidance literature:: With triphenylphosphine; In ethyl acetate; at 80 ℃; for 20h;

Reference yield:

: 145819-52-9
(5S,6R)-2,2'-anhydro-1-(3'-bromo-3'-deoxy-5'-O-trityl-β-D-arabinofuranosyl)-5,6-epoxy-5,6-dihydrothymine

: 115913-84-3
1-(2,3-epoxy-5-O-trityl-β-D-lyxo-pentofuranosyl)thymine

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / Ph₃P / ethyl acetate / 20 h / 80 °C

2: 93 percent / NaOH / acetone / 0.33 h

With sodium hydroxide; triphenylphosphine; In ethyl acetate; acetone;