(S)-4-[N-(tert-butyloxycarbonyl)-N-benzyl]amino-5-methylhexanal dimethyl acetal

Base Information

Chemical Name:(S)-4-[N-(tert-butyloxycarbonyl)-N-benzyl]amino-5-methylhexanal dimethyl acetal
CAS No.:257861-38-4
Molecular Formula:C₂₁H₃₅NO₄
Molecular Weight:365.513
Hs Code.:

Synonyms:(S)-4-[N-(tert-butyloxycarbonyl)-N-benzyl]amino-5-methylhexanal dimethyl acetal

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Chemical Property of (S)-4-[N-(tert-butyloxycarbonyl)-N-benzyl]amino-5-methylhexanal dimethyl acetal

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Technology Process of (S)-4-[N-(tert-butyloxycarbonyl)-N-benzyl]amino-5-methylhexanal dimethyl acetal

There total 5 articles about (S)-4-[N-(tert-butyloxycarbonyl)-N-benzyl]amino-5-methylhexanal dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22483-21-2
isobutylidenebenzylamine

: 257861-38-4
(S)-4-[N-(tert-butyloxycarbonyl)-N-benzyl]amino-5-methylhexanal dimethyl acetal

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent

2: Et₃N / tetrahydrofuran

3: pyridine; DMAP

4: p-TsOH

With pyridine; dmap; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; 1: Addition / 2: tert-butoxycarbonylation / 3: Acetylation / 4: acetalization;
DOI:10.1021/ja9933487

Reference yield:

: 257861-34-0
(E)-(4S)-4-(N-benzyl)amino-1-[(1R,2R)-2-hydroxy-1,2-dicyclohexylethyl]oxy-5-methyl-1-hexene

: 257861-38-4
(S)-4-[N-(tert-butyloxycarbonyl)-N-benzyl]amino-5-methylhexanal dimethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / tetrahydrofuran

2: pyridine; DMAP

3: p-TsOH

With pyridine; dmap; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; 1: tert-butoxycarbonylation / 2: Acetylation / 3: acetalization;
DOI:10.1021/ja9933487

Reference yield:

: Benzyl-[(E)-(S)-4-((1R,2R)-1,2-dicyclohexyl-2-hydroxy-ethoxy)-1-isopropyl-but-3-enyl]-carbamic acid tert-butyl ester

: 257861-38-4
(S)-4-[N-(tert-butyloxycarbonyl)-N-benzyl]amino-5-methylhexanal dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; DMAP

2: p-TsOH

With pyridine; dmap; toluene-4-sulfonic acid; 1: Acetylation / 2: acetalization;
DOI:10.1021/ja9933487