diethyl N-(4'-methoxyphenyl)-N-(2-chloro)phenylthioacetyl-aminomalonate

Base Information

Chemical Name:diethyl N-(4'-methoxyphenyl)-N-(2-chloro)phenylthioacetyl-aminomalonate
CAS No.:221910-50-5
Molecular Formula:C₂₂H₂₄ClNO₆S
Molecular Weight:465.955
Hs Code.:

Synonyms:diethyl N-(4'-methoxyphenyl)-N-(2-chloro)phenylthioacetyl-aminomalonate

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Chemical Property of diethyl N-(4'-methoxyphenyl)-N-(2-chloro)phenylthioacetyl-aminomalonate

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Technology Process of diethyl N-(4'-methoxyphenyl)-N-(2-chloro)phenylthioacetyl-aminomalonate

There total 6 articles about diethyl N-(4'-methoxyphenyl)-N-(2-chloro)phenylthioacetyl-aminomalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 221910-49-2
diethyl N-(4'-methoxyphenyl)-1-phenylthioacetyl-aminomalonate

: 221910-50-5
diethyl N-(4'-methoxyphenyl)-N-(2-chloro)phenylthioacetyl-aminomalonate

Guidance literature:: With sulfuryl dichloride; In dichloromethane; at 0 ℃;

Reference yield:

: 7031-27-8
(phenylthio)acetic acid chloride

: 221910-50-5
diethyl N-(4'-methoxyphenyl)-N-(2-chloro)phenylthioacetyl-aminomalonate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

2: 94 percent / sulfuryl chloride / CH₂Cl₂ / 0 °C

With pyridine; sulfuryl dichloride; In dichloromethane;

Reference yield:

: 103-04-8
(phenylthio)acetic acid

: 221910-50-5
diethyl N-(4'-methoxyphenyl)-N-(2-chloro)phenylthioacetyl-aminomalonate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / phosphorus trichloride / Heating

2: 87 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

3: 94 percent / sulfuryl chloride / CH₂Cl₂ / 0 °C

With pyridine; sulfuryl dichloride; phosphorus trichloride; In dichloromethane;