3-Methylmercapto-6-(4-acetylaminobenzyl)-2,5-dihydro-1,2,4-triazin-5-on

Base Information

Chemical Name:3-Methylmercapto-6-(4-acetylaminobenzyl)-2,5-dihydro-1,2,4-triazin-5-on
CAS No.:77441-97-5
Molecular Formula:C₁₃H₁₄N₄O₂S
Molecular Weight:290.346
Hs Code.:

Synonyms:3-Methylmercapto-6-(4-acetylaminobenzyl)-2,5-dihydro-1,2,4-triazin-5-on

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Methylmercapto-6-(4-acetylaminobenzyl)-2,5-dihydro-1,2,4-triazin-5-on

Chemical Property:

Purity/Quality:

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Technology Process of 3-Methylmercapto-6-(4-acetylaminobenzyl)-2,5-dihydro-1,2,4-triazin-5-on

There total 5 articles about 3-Methylmercapto-6-(4-acetylaminobenzyl)-2,5-dihydro-1,2,4-triazin-5-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.7%

: 77441-95-3
2-Thio-5-(4-acetylaminobenzyl)-6-azauracil

: 74-88-4
methyl iodide

: 77441-97-5
3-Methylmercapto-6-(4-acetylaminobenzyl)-2,5-dihydro-1,2,4-triazin-5-on

Guidance literature:: With sodium carbonate; In water; for 10h;

Reference yield:

: 77441-94-2
2-Thio-5-(4-aminobenzyl)-6-azauracil

: 77441-97-5
3-Methylmercapto-6-(4-acetylaminobenzyl)-2,5-dihydro-1,2,4-triazin-5-on

Guidance literature:: Multi-step reaction with 2 steps

1: 88.3 percent / ethyl acetate / 0.33 h / Heating

2: 94.7 percent / Na₂CO₃ / H₂O / 10 h

With sodium carbonate; In water; ethyl acetate;

Reference yield:

: 77441-93-1
C₁₀H₁₂N₄O₂S

: 77441-97-5
3-Methylmercapto-6-(4-acetylaminobenzyl)-2,5-dihydro-1,2,4-triazin-5-on

Guidance literature:: Multi-step reaction with 3 steps

1: 87.8 percent / Na₂CO₃ / H₂O / 3 h / Heating

2: 88.3 percent / ethyl acetate / 0.33 h / Heating

3: 94.7 percent / Na₂CO₃ / H₂O / 10 h

With sodium carbonate; In water; ethyl acetate;