C₁₉H₂₃IN₂O₄

Base Information

Chemical Name:C₁₉H₂₃IN₂O₄
CAS No.:1374442-50-8
Molecular Formula:C₁₉H₂₃IN₂O₄
Molecular Weight:470.307
Hs Code.:

C<sub>19</sub>H<sub>23</sub>IN<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₉H₂₃IN₂O₄

Suppliers and Price of C₁₉H₂₃IN₂O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₉H₂₃IN₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₉H₂₃IN₂O₄

There total 5 articles about C₁₉H₂₃IN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 74-85-1
ethene

: 1374442-44-0
C₁₇H₁₉IN₂O₄

: 1374442-50-8
C₁₉H₂₃IN₂O₄

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 20 ℃; under 760.051 Torr;
DOI:10.1002/ejoc.201101744

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 1374442-50-8
C₁₉H₂₃IN₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; iodine; acetic acid / 21 h / 70 °C / Inert atmosphere

2: thionyl chloride / 24 h / 0 - 20 °C / Inert atmosphere

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 24 h / 0 - 20 °C / pH 9 / Inert atmosphere

4: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 20 °C / 760.05 Torr

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; thionyl chloride; sulfuric acid; iodine; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.201101744

Reference yield:

: 23235-02-1,23235-04-3,23234-80-2
N-Acetyl-α-propargylglycine

: 1374442-50-8
C₁₉H₂₃IN₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 24 h / 0 - 20 °C / pH 9 / Inert atmosphere

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 20 °C / 760.05 Torr

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.201101744