Technology Process of C26H34ClN6O4P
There total 11 articles about C26H34ClN6O4P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
at 60 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: dipyridinium dichromate / dichloromethane / 2 h / 20 °C / molecular sieve
2: dichloromethane / 0.5 h / 20 °C
3: hydrogen / palladium 10% on activated carbon / methanol / 20 °C
4: sulfuric acid; guanidine nitrate / 3 h / 20 °C
5: trifluoroacetic acid / iso-butanol / 18 h / 100 °C
6: potassium carbonate; methanol / 0.25 h / 60 °C / Capped vial
7: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 2 h / 20 °C
8: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 60 °C
With
methanol; dipyridinium dichromate; dimethylsulfide borane complex; sulfuric acid; hydrogen; guanidine nitrate; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; trifluoroacetic acid;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; iso-butanol;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: dichloromethane / 0.5 h / 20 °C
2: hydrogen / palladium 10% on activated carbon / methanol / 20 °C
3: sulfuric acid; guanidine nitrate / 3 h / 20 °C
4: trifluoroacetic acid / iso-butanol / 18 h / 100 °C
5: potassium carbonate; methanol / 0.25 h / 60 °C / Capped vial
6: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 2 h / 20 °C
7: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 60 °C
With
methanol; dimethylsulfide borane complex; sulfuric acid; hydrogen; guanidine nitrate; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; trifluoroacetic acid;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; iso-butanol;