tert-Butyl (1-(2-bromophenyl)ethyl)carbamate

Base Information

Chemical Name:tert-Butyl (1-(2-bromophenyl)ethyl)carbamate
CAS No.:1086391-99-2
Molecular Formula:C₁₃H₁₈BrNO₂
Molecular Weight:300.195
Hs Code.:
DSSTox Substance ID:DTXSID001161629
Mol file:1086391-99-2.mol

Synonyms:tert-Butyl (1-(2-bromophenyl)ethyl)carbamate;1086391-99-2;108639-99-2;tert-butyl N-[1-(2-bromophenyl)ethyl]carbamate;[1-(2-Bromo-phenyl)-ethyl]-carbamic acid tert-butyl ester;CarbaMic acid, [1-(2-broMophenyl)ethyl]-, 1,1-diMethylethyl ester;13,15,28-Trioxa-14-phosphatetrapentaconta-9,18-dienoic acid,12,16-dihexyl-14-hydroxy-27-oxo-, hexacosyl ester, 14-oxide,[R-[R*,R*-(Z,Z)]]-;SCHEMBL1343848;RMNWPYMNQJCFTE-UHFFFAOYSA-N;DTXSID001161629;AKOS013099193;SB30539;SB30595;SB31471;BS-50506;CS-0277069;E79839;EN300-6287658;Carbamic acid, N-[1-(2-bromophenyl)ethyl]-, 1,1-dimethylethyl ester

Suppliers and Price of tert-Butyl (1-(2-bromophenyl)ethyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
tert-Butyl(1-(2-bromophenyl)ethyl)carbamate
1g
$ 400.00

Total 7 raw suppliers

Chemical Property of tert-Butyl (1-(2-bromophenyl)ethyl)carbamate

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:299.05209
Heavy Atom Count:17
Complexity:263

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl(1-(2-bromophenyl)ethyl)carbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C1=CC=CC=C1Br)NC(=O)OC(C)(C)C

Technology Process of tert-Butyl (1-(2-bromophenyl)ethyl)carbamate

There total 2 articles about tert-Butyl (1-(2-bromophenyl)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 113899-55-1
rac-2'-bromo-α-methylbenzylamine

: 1086391-99-2
rac-N-Boc-2'-bromo-α-methylbenzylamine

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 24h;
DOI:10.1002/anie.201708453

Reference yield:

: 2142-69-0
2-bromophenyl methyl ketone

: 1086391-99-2
rac-N-Boc-2'-bromo-α-methylbenzylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonia; titanium(IV) isopropylate / ethanol / 18 h / 20 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 24 h / 0 - 20 °C

With titanium(IV) isopropylate; ammonia; triethylamine; In ethanol; dichloromethane;
DOI:10.1002/anie.201708453