2-[2-(4-nitrophenyl)ethyl]-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro naphthalen-2-yl)-1,3,4-oxadiazole

Base Information

Chemical Name:2-[2-(4-nitrophenyl)ethyl]-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro naphthalen-2-yl)-1,3,4-oxadiazole
CAS No.:1022171-46-5
Molecular Formula:C₂₄H₂₇N₃O₃
Molecular Weight:405.497
Hs Code.:

Synonyms:2-[2-(4-nitrophenyl)ethyl]-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro naphthalen-2-yl)-1,3,4-oxadiazole

Suppliers and Price of 2-[2-(4-nitrophenyl)ethyl]-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro naphthalen-2-yl)-1,3,4-oxadiazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-[2-(4-nitrophenyl)ethyl]-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro naphthalen-2-yl)-1,3,4-oxadiazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-[2-(4-nitrophenyl)ethyl]-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro naphthalen-2-yl)-1,3,4-oxadiazole

There total 4 articles about 2-[2-(4-nitrophenyl)ethyl]-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro naphthalen-2-yl)-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.9%

: 34547-21-2
3-(4-nitro-phenyl)-propionic acid hydrazide

: C₁₇H₂₅NO*ClH

: 1022171-46-5
2-[2-(4-nitrophenyl)ethyl]-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro naphthalen-2-yl)-1,3,4-oxadiazole

Guidance literature:: In ethanol; at 95 ℃; for 8h; Temperature;

Reference yield: 35.0%

: 34547-21-2
3-(4-nitro-phenyl)-propionic acid hydrazide

: 104224-50-2
5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphtholyl chloride

: 1022171-46-5
2-[2-(4-nitrophenyl)ethyl]-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro naphthalen-2-yl)-1,3,4-oxadiazole

Guidance literature:: 3-(4-nitro-phenyl)-propionic acid hydrazide; 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphtholyl chloride; With trichlorophosphate; at 150 ℃; for 1h; Microwave irradiation; Sealed tube;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: 5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalene-2-carbonitrile

: 1022171-46-5
2-[2-(4-nitrophenyl)ethyl]-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro naphthalen-2-yl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride / 48 h / 3 - 30 °C

2: ethanol / 8 h / 95 °C

With acetyl chloride; In ethanol;