P-[2-(dicyclohexylphosphino)phenyl]-N,N-diisopropyl-P-phenylphosphinic amide

Base Information

Chemical Name:P-[2-(dicyclohexylphosphino)phenyl]-N,N-diisopropyl-P-phenylphosphinic amide
CAS No.:1198339-47-7
Molecular Formula:C₃₀H₄₅NOP₂
Molecular Weight:497.641
Hs Code.:

Synonyms:P-[2-(dicyclohexylphosphino)phenyl]-N,N-diisopropyl-P-phenylphosphinic amide

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Chemical Property of P-[2-(dicyclohexylphosphino)phenyl]-N,N-diisopropyl-P-phenylphosphinic amide

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Technology Process of P-[2-(dicyclohexylphosphino)phenyl]-N,N-diisopropyl-P-phenylphosphinic amide

There total 3 articles about P-[2-(dicyclohexylphosphino)phenyl]-N,N-diisopropyl-P-phenylphosphinic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 131173-04-1
N,N-Di-isopropyl-P,P-diphenylphosphinic amide

: 16523-54-9
chlorodicyclohexylphosphane

: 1198339-47-7
P-[2-(dicyclohexylphosphino)phenyl]-N,N-diisopropyl-P-phenylphosphinic amide

Guidance literature:: N,N-Di-isopropyl-P,P-diphenylphosphinic amide; With sec.-butyllithium; In tetrahydrofuran; at -70 - -40 ℃; Inert atmosphere;

chlorodicyclohexylphosphane; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1055/s-0029-1216897

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1198339-47-7
P-[2-(dicyclohexylphosphino)phenyl]-N,N-diisopropyl-P-phenylphosphinic amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine

2: N,N,N,N,-tetramethylethylenediamine; n-butyllithium

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; triethylamine;
DOI:10.1021/acscatal.5b01490

Reference yield:

: 108-18-9
diisopropylamine

: 1198339-47-7
P-[2-(dicyclohexylphosphino)phenyl]-N,N-diisopropyl-P-phenylphosphinic amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: dihydrogen peroxide / Inert atmosphere

2.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / Inert atmosphere

2.2: Inert atmosphere

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; dihydrogen peroxide;
DOI:10.1039/c8dt01018h