trans-2-[3-(2-Hydroxypropylsulfonyl)-4-n-propoxy-5-benzyloxyphenyl]-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran

Base Information

• Chemical Name: trans-2-[3-(2-Hydroxypropylsulfonyl)-4-n-propoxy-5-benzyloxyphenyl]-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran
• CAS No.: 134169-28-1
• Molecular Formula: C₃₂H₄₀O₉S
• Molecular Weight: 600.73

Synonyms:trans-2-[3-(2-Hydroxypropylsulfonyl)-4-n-propoxy-5-benzyloxyphenyl]-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran

Chemical Property of trans-2-[3-(2-Hydroxypropylsulfonyl)-4-n-propoxy-5-benzyloxyphenyl]-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran

Chemical Property:

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Technology Process of trans-2-[3-(2-Hydroxypropylsulfonyl)-4-n-propoxy-5-benzyloxyphenyl]-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran

There total 13 articles about trans-2-[3-(2-Hydroxypropylsulfonyl)-4-n-propoxy-5-benzyloxyphenyl]-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

trans-2-[3-(2-hydroxy-n-propylsulfonyl)-4-n propoxy-5-(3-hydroxy-n-propoxy)phenyl]-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran (134169-30-5,134236-05-8) → trans-2-[3-(2-Hydroxypropylsulfonyl)-4-n-propoxy-5-benzyloxyphenyl]-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran (134169-28-1)

Guidance literature:

In tetrahydrofuran; methanol; dichloromethane; acetic acid;

Reference yield: 75.0%

acetaldehyde (75-07-0,9002-91-9) + trans-2-(3-benzyloxy-4-propoxy-5-methylsulfonylphenyl)-5-(3,4,5-trimethoxyphenyl)-tetrahydrofuran (134186-90-6) → (-)-trans-(2S,5S)-2-<3-<((2R,S)-2-hydroxypropyl)-sulfonyl>-4-n-propyl-5-(benzyloxy)phenyl>-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran (134169-28-1,134236-02-5,134236-03-6)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; cyclohexane; at -70 ℃; for 0.166667h;

DOI:10.1021/jm00097a005

Reference yield:

(-)-trans-(2S,5S)-2-(3-Methylsulfonyl-4-n-propoxy-5-benzyloxyphenyl)-5-(3,4,5-trimethoxyphenyl) tetrahydrofuran → trans-2-[3-(2-Hydroxypropylsulfonyl)-4-n-propoxy-5-benzyloxyphenyl]-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran (134169-28-1)

Guidance literature:

With diisopropylamine; In tetrahydrofuran; dichloromethane; cyclohexane;

upstream raw materials:

acetaldehyde

trans-2-(3-benzyloxy-4-propoxy-5-methylsulfonylphenyl)-5-(3,4,5-trimethoxyphenyl)-tetrahydrofuran

3-benzyloxy-4-hydroxybenzaldehyde

3-bromo-4-hydroxy-5-benzyloxybenzaldehyde

Downstream raw materials:

3-((S)-2-Hydroxy-propane-1-sulfonyl)-2-propoxy-5-[(2S,5S)-5-(3,4,5-trimethoxy-phenyl)-tetrahydro-furan-2-yl]-phenol

3-((R)-2-Hydroxy-propane-1-sulfonyl)-2-propoxy-5-[(2S,5S)-5-(3,4,5-trimethoxy-phenyl)-tetrahydro-furan-2-yl]-phenol

(-)-trans-(2S,5S)-2-<3-<((2S)-2-hydroxypropyl)sulfonyl>-4-n-propoxy-5-(3-hydroxypropoxy)phenyl>-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran

(-)-trans-(2S,5S)-2-<3-<((2R)-2-hydroxypropyl)sulfonyl>-4-n-propoxy-5-(3-hydroxypropoxy)phenyl>-5-(3,4,5-trimethoxyphenyl)tetrahydrofuran

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