Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)]B(C₆H₃(CF₃)2)4

Base Information

• Chemical Name: Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)]B(C₆H₃(CF₃)2)4
• CAS No.: 160498-16-8
• Molecular Formula: C₁₆H₁₅N₂OPd*C₃₂H₁₂BF₂₄
• Molecular Weight: 1220.95

Synonyms:Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)]B(C₆H₃(CF₃)2)4

Chemical Property of Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)]B(C₆H₃(CF₃)2)4

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Technology Process of Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)]B(C₆H₃(CF₃)2)4

There total 3 articles about Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Pd(C₁₂H₈N₂)(CH₃CO)(C₂H₄)]B(C₆H₃(CF₃)2)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

ethene (74-85-1) + [Pd(CH3)(CO)(1,10-phenanthroline)][B(3,5-(CF3)2-C6H3)4] (160498-14-6) → Pd(C12H8N2)(CH3CO)(C2H4)(1+)*B(C6H3(CF3)2)4(1-)=[Pd(C12H8N2)(CH3CO)(C2H4)]B(C6H3(CF3)2)4 (160498-16-8)

Guidance literature:

In dichloromethane-d2; -66°C, excess of ethylene (8 equiv); holding the solution under vacuum at -78°C for 15 h; Kinetics;

DOI:10.1021/ja00108a034

Reference yield: 78.0%

ethene (74-85-1) + [Pd(CH3)(CO)(1,10-phenanthroline)][B(3,5-(CF3)2-C6H3)4] (160498-14-6) → (C12H8N2)Pd(CH3)(C2H4)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(CH3)(C2H4)]B(C6H3(CF3)2)4 (160498-12-4) + (C12H8N2)Pd(C(O)CH3)(C2H4)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(C(O)CH3)(C2H4)]B(C6H3(CF3)2)4 (160498-16-8) + (C12H8N2)Pd(CH2CH2C(CH3)O)(1+)*B(C6H3(CF3)2)4(1-) = [(C12H8N2)Pd(CH2CH2C(CH3)O)]B(C6H3(CF3)2)4 + (C12H8N2)Pd(CH2CH2C(O)CH3)(C2H4)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(CH2CH2C(O)CH3)(C2H4)]B(C6H3(CF3)2)4 (160498-05-5) + (C12H8N2)Pd(C(O)CH2CH2C(O)CH3)(C2H4)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(C(O)CH2CH2C(O)CH3)(C2H4)]B(C6H3(CF3)2)4 (160498-06-6)

Guidance literature:

In dichloromethane-d2; (Ar); -78°C, 4 h; vac. drying (-78°C, overnight); Kinetics;

DOI:10.1021/ja953276t

Reference yield:

ethene (74-85-1) + [Pd(CH3)(CO)(1,10-phenanthroline)][B(3,5-(CF3)2-C6H3)4] (160498-14-6) → (C12H8N2)Pd(CH3)(C2H4)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(CH3)(C2H4)]B(C6H3(CF3)2)4 (160498-12-4) + (C12H8N2)Pd(C(O)CH3)(C2H4)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(C(O)CH3)(C2H4)]B(C6H3(CF3)2)4 (160498-16-8) + (C12H8N2)Pd(CH2CH2C(CH3)O)(1+)*B(C6H3(CF3)2)4(1-) = [(C12H8N2)Pd(CH2CH2C(CH3)O)]B(C6H3(CF3)2)4 + (C12H8N2)Pd(C(O)CH2CH2C(CH3)O)(1+)*B(C6H3(CF3)2)4(1-) = [(C12H8N2)Pd(C(O)CH2CH2C(CH3)O)]B(C6H3(CF3)2)4 + (C12H8N2)Pd(CH2CH2C(O)CH3)(C2H4)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(CH2CH2C(O)CH3)(C2H4)]B(C6H3(CF3)2)4 (160498-05-5)

Guidance literature:

In dichloromethane-d2; (Ar); -78°C, 4 h; vac. drying (-78.degrre.C, overnight);

DOI:10.1021/ja953276t

upstream raw materials:

ethene

[Pd(CH₃)(CO)(1,10-phenanthroline)][B(3,5-(CF₃)2-C₆H₃)4]

Downstream raw materials:

Pd(C₁₂H₈N₂)(CH₂CH₂COCH₃)(C₂H₄)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Pd(C₁₂H₈N₂)(CH₂CH₂COCH₃)(C₂H₄)]B(C₆H₃(CF₃)2)4

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