(R)-(-)-3-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-1-<(4-methylphenyl)sulfonyloxy>-2-propanol

Base Information

• Chemical Name: (R)-(-)-3-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-1-<(4-methylphenyl)sulfonyloxy>-2-propanol
• CAS No.: 144024-34-0
• Molecular Formula: C₂₅H₂₅NO₇S₂
• Molecular Weight: 515.608

Synonyms:(R)-(-)-3-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-1-<(4-methylphenyl)sulfonyloxy>-2-propanol

Chemical Property of (R)-(-)-3-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-1-<(4-methylphenyl)sulfonyloxy>-2-propanol

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Technology Process of (R)-(-)-3-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-1-<(4-methylphenyl)sulfonyloxy>-2-propanol

There total 2 articles about (R)-(-)-3-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-1-<(4-methylphenyl)sulfonyloxy>-2-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

(R)-3-tosyloxy-1,2-propanediol (41274-09-3) + 4-<1-(4-methylphenyl)sulfonyl-3-pyrrolyl>-4-oxobutanal (144024-32-8) → (R)-(+)-2-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-3-<(4-methylphenyl)sulfonyloxy>-1-propanol (144024-35-1) + (R)-(-)-3-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-1-<(4-methylphenyl)sulfonyloxy>-2-propanol (144024-34-0)

Guidance literature:

With sulfuric acid; In dichloromethane; for 3h; Heating;

DOI:10.1248/cpb.40.2353

Reference yield: 67.0%

(R)-3-tosyloxy-1,2-propanediol (41274-09-3) + 4,4-dimethoxy-1-<1-(4-methylphenyl)sulfonyl-3-pyrrolyl>-1-butanone (144024-31-7) → (R)-(+)-2-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-3-<(4-methylphenyl)sulfonyloxy>-1-propanol (144024-35-1) + (R)-(-)-3-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-1-<(4-methylphenyl)sulfonyloxy>-2-propanol (144024-34-0)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 3h; Heating;

DOI:10.1248/cpb.40.2353

Reference yield: 98.0%

(R)-(-)-3-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-1-<(4-methylphenyl)sulfonyloxy>-2-propanol (144024-34-0) + isopropylamine (75-31-0) → (S)-(-)-1-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-3-(2-propylamino)-2-propanol (144024-36-2)

Guidance literature:

for 26h; Heating;

DOI:10.1248/cpb.40.2353

upstream raw materials:

(R)-3-tosyloxy-1,2-propanediol

4-<1-(4-methylphenyl)sulfonyl-3-pyrrolyl>-4-oxobutanal

4,4-dimethoxy-1-<1-(4-methylphenyl)sulfonyl-3-pyrrolyl>-1-butanone

Downstream raw materials:

(S)-(-)-1-<1-(4-methylphenyl)sulfonyl-4-indolyloxy>-3-(2-propylamino)-2-propanol

(S)-pindolol

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