N-<4-O--3-nitrobenzyloxycarbonyl>glycine

Base Information

Chemical Name:N-<4-O--3-nitrobenzyloxycarbonyl>glycine
CAS No.:228412-63-3
Molecular Formula:C₂₃H₂₆N₂O₁₆
Molecular Weight:586.463
Hs Code.:

N-<4-O-<methyl (2,3,4-tri-O-acetyl-β-D-glucopyranosyl)uronate>-3-nitrobenzyloxycarbonyl>glycine

Synonyms:N-<4-O--3-nitrobenzyloxycarbonyl>glycine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<4-O--3-nitrobenzyloxycarbonyl>glycine

Chemical Property:

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Technology Process of N-<4-O--3-nitrobenzyloxycarbonyl>glycine

There total 2 articles about N-<4-O--3-nitrobenzyloxycarbonyl>glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 56-40-6,18875-39-3,25718-94-9
glycine

: 148580-01-2
(2S,3S,4S,5R,6S)-3,4,5-Triacetoxy-6-[2-nitro-4-(4-nitro-phenoxycarbonyloxymethyl)-phenoxy]-tetrahydro-pyran-2-carboxylic acid methyl ester

: 228412-63-3
N-<4-O--3-nitrobenzyloxycarbonyl>glycine

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 18h; Ambient temperature;

Reference yield:

: 148579-94-6
(25,3R,45,55,65)-2-(4-(hydroxymethyl)-2-nitrophenoxy)-6-(methoxycarbonyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 228412-63-3
N-<4-O--3-nitrobenzyloxycarbonyl>glycine

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / acetonitrile / 2 h / 20 °C

2: Et₃N / acetonitrile; dimethylformamide / 16 h / 20 °C

With triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm010352w