L-pGlu-L-Phe-Pyrr

Base Information

Chemical Name:L-pGlu-L-Phe-Pyrr
CAS No.:76597-70-1
Molecular Formula:C₁₈H₂₃N₃O₃
Molecular Weight:329.399
Hs Code.:

Synonyms:L-pGlu-L-Phe-Pyrr

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Chemical Property of L-pGlu-L-Phe-Pyrr

Chemical Property:

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Technology Process of L-pGlu-L-Phe-Pyrr

There total 3 articles about L-pGlu-L-Phe-Pyrr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 76597-70-1
L-pGlu-L-Phe-Pyrr

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) N-methylmorpholine, isobutyl chloroformate (IBCF) / 1.) ethyl acetate, -35 deg C, 7 min, 2.) ethyl acetate, RT, overnight

2: H₂, 3 N HCl / 5percent Pd/C / methanol / 1 h / 517.1 Torr / Ambient temperature

3: 1.) N-methylmorpholine, isobutyl chloroformate / 1.) ethyl acetate, -20 deg C, 12 min, 2.) ethyl acetate, RT, overnight

4: 56 percent / H₂ / 5percent Pd/C / methanol; acetic acid / 0.08 h / 258.6 Torr

With 4-methyl-morpholine; hydrogenchloride; hydrogen; isobutyl chloroformate; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1021/jm00136a003

Reference yield:

: 56414-67-6
((S)-1-Benzyl-2-oxo-2-pyrrolidin-1-yl-ethyl)-carbamic acid benzyl ester

: 76597-70-1
L-pGlu-L-Phe-Pyrr

Guidance literature:: Multi-step reaction with 3 steps

1: H₂, 3 N HCl / 5percent Pd/C / methanol / 1 h / 517.1 Torr / Ambient temperature

2: 1.) N-methylmorpholine, isobutyl chloroformate / 1.) ethyl acetate, -20 deg C, 12 min, 2.) ethyl acetate, RT, overnight

3: 56 percent / H₂ / 5percent Pd/C / methanol; acetic acid / 0.08 h / 258.6 Torr

With 4-methyl-morpholine; hydrogenchloride; hydrogen; isobutyl chloroformate; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1021/jm00136a003

Reference yield:

: 137137-81-6
L-Phe-Pyrr*HCl

: 76597-70-1
L-pGlu-L-Phe-Pyrr

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-methylmorpholine, isobutyl chloroformate / 1.) ethyl acetate, -20 deg C, 12 min, 2.) ethyl acetate, RT, overnight

2: 56 percent / H₂ / 5percent Pd/C / methanol; acetic acid / 0.08 h / 258.6 Torr

With 4-methyl-morpholine; hydrogen; isobutyl chloroformate; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1021/jm00136a003