3-(2,4-dichlorophenyl)-N¹-(4-fluorophenethyl)-N⁵-hydroxypentanediamide

Base Information

Chemical Name:3-(2,4-dichlorophenyl)-N¹-(4-fluorophenethyl)-N⁵-hydroxypentanediamide
CAS No.:1551577-31-1
Molecular Formula:C₁₉H₁₉Cl₂FN₂O₃
Molecular Weight:413.276
Hs Code.:

3-(2,4-dichlorophenyl)-N<SUP>1</SUP>-(4-fluorophenethyl)-N<SUP>5</SUP>-hydroxypentanediamide

Synonyms:3-(2,4-dichlorophenyl)-N¹-(4-fluorophenethyl)-N⁵-hydroxypentanediamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2,4-dichlorophenyl)-N¹-(4-fluorophenethyl)-N⁵-hydroxypentanediamide

Chemical Property:

Purity/Quality:

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Technology Process of 3-(2,4-dichlorophenyl)-N¹-(4-fluorophenethyl)-N⁵-hydroxypentanediamide

There total 6 articles about 3-(2,4-dichlorophenyl)-N¹-(4-fluorophenethyl)-N⁵-hydroxypentanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1551577-66-2
methyl 3-(2,4-dichlorophenyl)-5-((4-fluorophenethyl)amino)-5-oxopentanoate

: 1551577-31-1
3-(2,4-dichlorophenyl)-N¹-(4-fluorophenethyl)-N⁵-hydroxypentanediamide

Guidance literature:: With potassium cyanide; hydroxylamine; In tetrahydrofuran; methanol; water; at 20 ℃;
DOI:10.1016/j.bmc.2013.11.053

Reference yield:

: C₁₃H₉Cl₂F₃O₅

: 1551577-31-1
3-(2,4-dichlorophenyl)-N¹-(4-fluorophenethyl)-N⁵-hydroxypentanediamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / 0 - 20 °C

2: benzotriazol-1-ol; 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

3: potassium cyanide; hydroxylamine / tetrahydrofuran; water; methanol / 20 °C

With 4-methyl-morpholine; potassium cyanide; hydroxylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.bmc.2013.11.053

Reference yield:

: 1551577-02-6
tetramethyl 2-(2,4-dichlorophenyl)propane-1,1,3,3-tetracarboxylate

: 1551577-31-1
3-(2,4-dichlorophenyl)-N¹-(4-fluorophenethyl)-N⁵-hydroxypentanediamide

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride; water / Reflux

2: chloroform / 0 - 20 °C

3: triethylamine / 0 - 20 °C

4: benzotriazol-1-ol; 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

5: potassium cyanide; hydroxylamine / tetrahydrofuran; water; methanol / 20 °C

With 4-methyl-morpholine; hydrogenchloride; potassium cyanide; water; hydroxylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; water;
DOI:10.1016/j.bmc.2013.11.053