(4-bromo-2-methoxy-6-nitrophenyl)iminocarbonic acid-bis-(tert-butyl ester)

Base Information

Chemical Name:(4-bromo-2-methoxy-6-nitrophenyl)iminocarbonic acid-bis-(tert-butyl ester)
CAS No.:1426822-21-0
Molecular Formula:C₁₇H₂₃BrN₂O₇
Molecular Weight:447.283
Hs Code.:

Synonyms:(4-bromo-2-methoxy-6-nitrophenyl)iminocarbonic acid-bis-(tert-butyl ester)

Suppliers and Price of (4-bromo-2-methoxy-6-nitrophenyl)iminocarbonic acid-bis-(tert-butyl ester)

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Chemical Property of (4-bromo-2-methoxy-6-nitrophenyl)iminocarbonic acid-bis-(tert-butyl ester)

Chemical Property:

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Technology Process of (4-bromo-2-methoxy-6-nitrophenyl)iminocarbonic acid-bis-(tert-butyl ester)

There total 3 articles about (4-bromo-2-methoxy-6-nitrophenyl)iminocarbonic acid-bis-(tert-butyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77333-45-0
4-bromo-2-methoxy-6-nitrobenzenamine

: 24424-99-5
di-tert-butyl dicarbonate

: 1426822-21-0
(4-bromo-2-methoxy-6-nitrophenyl)iminocarbonic acid-bis-(tert-butyl ester)

Guidance literature:: With dmap; In dichloromethane; at 20 ℃;

Reference yield:

: 16554-45-3
2-methoxy-6-nitroaniline

: 1426822-21-0
(4-bromo-2-methoxy-6-nitrophenyl)iminocarbonic acid-bis-(tert-butyl ester)

Guidance literature:: Multi-step reaction with 2 steps

1: bromine; sodium acetate / acetic acid / 0.25 h / 20 °C

2: dmap / dichloromethane / 20 °C

With dmap; bromine; sodium acetate; In dichloromethane; acetic acid;

Reference yield:

: 603-85-0
2-Amino-3-nitrophenol

: 1426822-21-0
(4-bromo-2-methoxy-6-nitrophenyl)iminocarbonic acid-bis-(tert-butyl ester)

Guidance literature:: Multi-step reaction with 3 steps

1: tetra-(n-butyl)ammonium iodide; sodium hydroxide / tetrahydrofuran; water / 20 °C

2: bromine; sodium acetate / acetic acid / 0.25 h / 20 °C

3: dmap / dichloromethane / 20 °C

With dmap; bromine; sodium acetate; tetra-(n-butyl)ammonium iodide; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; acetic acid;