3-(4-Chlorphenyl)-1,1-dimethyl-2-(methyl-4-chlorphenyl-sulfamoyl)-guanidin

Base Information

Chemical Name:3-(4-Chlorphenyl)-1,1-dimethyl-2-(methyl-4-chlorphenyl-sulfamoyl)-guanidin
CAS No.:124852-16-0
Molecular Formula:C₁₆H₁₈Cl₂N₄O₂S
Molecular Weight:401.317
Hs Code.:

Synonyms:3-(4-Chlorphenyl)-1,1-dimethyl-2-(methyl-4-chlorphenyl-sulfamoyl)-guanidin

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Chemical Property of 3-(4-Chlorphenyl)-1,1-dimethyl-2-(methyl-4-chlorphenyl-sulfamoyl)-guanidin

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Technology Process of 3-(4-Chlorphenyl)-1,1-dimethyl-2-(methyl-4-chlorphenyl-sulfamoyl)-guanidin

There total 2 articles about 3-(4-Chlorphenyl)-1,1-dimethyl-2-(methyl-4-chlorphenyl-sulfamoyl)-guanidin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 124852-02-4
3-(4-Chlorphenyl)-2-(4-chlorphenyl-sulfamoyl)-1,1-dimethylguanidin

: 74-88-4
methyl iodide

: 124852-16-0
3-(4-Chlorphenyl)-1,1-dimethyl-2-(methyl-4-chlorphenyl-sulfamoyl)-guanidin

Guidance literature:: With HCl-buffer; tetra(n-butyl)ammonium hydroxide; sodium carbonate; In dichloromethane; for 1h;

Reference yield:

: 106-47-8
4-chloro-aniline

: 124852-16-0
3-(4-Chlorphenyl)-1,1-dimethyl-2-(methyl-4-chlorphenyl-sulfamoyl)-guanidin

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / benzene / 2 h / Ambient temperature

2: 90 percent / Bu₄N⁽¹⁺⁾*OH^(1-), Na₂CO₃/HCl-buffer (pH=11.7) / CH₂Cl₂ / 1 h

With HCl-buffer; tetra(n-butyl)ammonium hydroxide; sodium carbonate; In dichloromethane; benzene;