4,4-di-p-chlorophenyl-1-hydroxy-2-methylthio-4,5-dihydroimidazole-5-thione

Base Information

Chemical Name:4,4-di-p-chlorophenyl-1-hydroxy-2-methylthio-4,5-dihydroimidazole-5-thione
CAS No.:144267-55-0
Molecular Formula:C₁₆H₁₂Cl₂N₂OS₂
Molecular Weight:383.322
Hs Code.:

Synonyms:4,4-di-p-chlorophenyl-1-hydroxy-2-methylthio-4,5-dihydroimidazole-5-thione

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Chemical Property of 4,4-di-p-chlorophenyl-1-hydroxy-2-methylthio-4,5-dihydroimidazole-5-thione

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Technology Process of 4,4-di-p-chlorophenyl-1-hydroxy-2-methylthio-4,5-dihydroimidazole-5-thione

There total 1 articles about 4,4-di-p-chlorophenyl-1-hydroxy-2-methylthio-4,5-dihydroimidazole-5-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 144267-42-5
2,5-dimethylthio-4,4-di-p-chlorophenyl-(4H)-imidazole-1-oxide

: 144267-55-0
4,4-di-p-chlorophenyl-1-hydroxy-2-methylthio-4,5-dihydroimidazole-5-thione

Guidance literature:: With sodium hydrogensulfide; In N,N-dimethyl-formamide; for 1h; Ambient temperature;
DOI:10.1016/S0040-4020(01)88250-8

Reference yield: 96.0%

: 144267-55-0
4,4-di-p-chlorophenyl-1-hydroxy-2-methylthio-4,5-dihydroimidazole-5-thione

: 112-67-4
n-hexadecanoyl chloride

: 144267-63-0
4,4-di-p-chlorophenyl-2-methylthio-1-palmitoyloxy-4,5-dihydroimidazole-5-thione

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1016/S0040-4020(01)88250-8

Reference yield:

: 144267-55-0
4,4-di-p-chlorophenyl-1-hydroxy-2-methylthio-4,5-dihydroimidazole-5-thione

: 144267-68-5
4,4-di-p-chlorophenyl-2-methylthio-5-n-pentadecylthio-(4H)-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

2: 97 percent / CDCl₃ / 0 °C / Irradiation

With pyridine; In chloroform-d1; dichloromethane;
DOI:10.1016/S0040-4020(01)88250-8