N'-(2-ethyl-3-methoxy-benzoyl)-hydrazinecarboxylic acid tert-butyl ester

Base Information

• Chemical Name: N'-(2-ethyl-3-methoxy-benzoyl)-hydrazinecarboxylic acid tert-butyl ester
• CAS No.: 740799-70-6
• Molecular Formula: C₁₅H₂₂N₂O₄
• Molecular Weight: 294.351
• Mol file: 740799-70-6.mol

Synonyms:N'-(2-ethyl-3-methoxy-benzoyl)-hydrazinecarboxylic acid tert-butyl ester

Chemical Property of N'-(2-ethyl-3-methoxy-benzoyl)-hydrazinecarboxylic acid tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N'-(2-ethyl-3-methoxy-benzoyl)-hydrazinecarboxylic acid tert-butyl ester

There total 1 articles about N'-(2-ethyl-3-methoxy-benzoyl)-hydrazinecarboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

t-butoxycarbonylhydrazine (870-46-2) + 2-ethyl-3-methoxybenzoyl chloride (180341-36-0) → N'-(2-ethyl-3-methoxy-benzoyl)-hydrazinecarboxylic acid tert-butyl ester (740799-70-6)

Guidance literature:

With potassium carbonate; In dichloromethane; water; at 0 - 20 ℃; for 18.5h;

Reference yield: 60.0%

N'-(2-ethyl-3-methoxy-benzoyl)-hydrazinecarboxylic acid tert-butyl ester (740799-70-6) + trifluoroacetic acid (76-05-1) → 2-ethyl-3-methoxy-benzoic acid hydrazide trifluoroacetate

Guidance literature:

N'-(2-ethyl-3-methoxy-benzoyl)-hydrazinecarboxylic acid tert-butyl ester; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 18h;

In diethyl ether; hexane; dichloromethane; for 1h;

upstream raw materials:

t-butoxycarbonylhydrazine

2-ethyl-3-methoxybenzoyl chloride