2-[2-(2-methoxyethoxy)ethoxy]ethyl 5-bromo-3-nitrobenzoate

Base Information

• Chemical Name: 2-[2-(2-methoxyethoxy)ethoxy]ethyl 5-bromo-3-nitrobenzoate
• CAS No.: 398119-24-9
• Molecular Formula: C₁₄H₁₈BrNO₇
• Molecular Weight: 392.203
• Mol file: 398119-24-9.mol

Synonyms:2-[2-(2-methoxyethoxy)ethoxy]ethyl 5-bromo-3-nitrobenzoate

Chemical Property of 2-[2-(2-methoxyethoxy)ethoxy]ethyl 5-bromo-3-nitrobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-[2-(2-methoxyethoxy)ethoxy]ethyl 5-bromo-3-nitrobenzoate

There total 1 articles about 2-[2-(2-methoxyethoxy)ethoxy]ethyl 5-bromo-3-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

triethylene glucol monomethyl ether (112-35-6,95507-80-5) + methyl 3-bromo-5-nitrobenzoate (6307-87-5) → 2-[2-(2-methoxyethoxy)ethoxy]ethyl 5-bromo-3-nitrobenzoate (398119-24-9)

Guidance literature:

With potassium carbonate; at 70 ℃; under 0.3 Torr;

DOI:10.1021/ja025698q

Reference yield: 86.0%

2-[2-(2-methoxyethoxy)ethoxy]ethyl 5-bromo-3-nitrobenzoate (398119-24-9) + 2-[2-(2-methoxyethoxy)ethoxy]ethyl 3,5-biethynylbenzoate (398119-23-8) → C46H54N2O19 (398119-25-0)

Guidance literature:

With copper(l) iodide; triethylamine; triphenylphosphine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; at 70 ℃; for 36h;

DOI:10.1021/jo010918o

Reference yield: 85.0%

C34H38O10 (545432-91-5) + 2-[2-(2-methoxyethoxy)ethoxy]ethyl 5-bromo-3-nitrobenzoate (398119-24-9) → C62H72N2O24

Guidance literature:

With copper(l) iodide; triethylamine; triphenylphosphine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In acetonitrile; at 65 ℃; for 36h;

DOI:10.1021/ja026957e

upstream raw materials:

triethylene glucol monomethyl ether

methyl 3-bromo-5-nitrobenzoate

Downstream raw materials:

C₄₆H₅₄N₂O₁₉

2-[2-(2-methoxyethoxy)ethoxy]ethyl 3-amino-5-ethynylbenzoate

C₄₆H₅₄N₂O₁₅H₄