C₂₆H₃₀Cl₂N₂O₅

Base Information

• Chemical Name: C₂₆H₃₀Cl₂N₂O₅
• CAS No.: 1430799-17-9
• Molecular Formula: C₂₆H₃₀Cl₂N₂O₅
• Molecular Weight: 521.441
• Mol file: 1430799-17-9.mol

Synonyms:C₂₆H₃₀Cl₂N₂O₅

Chemical Property of C₂₆H₃₀Cl₂N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₃₀Cl₂N₂O₅

There total 5 articles about C₂₆H₃₀Cl₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4,6-dichloro-5-methoxy-1,3-phenylene)bis(trimethylsilane) (1221589-81-6) → C26H30Cl2N2O5 (1430799-17-9)

Guidance literature:

Multi-step reaction with 3 steps

1: Iodine monochloride / dichloromethane / 20 °C / Cooling with ice

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 24.08 h / 80 °C / Inert atmosphere; Schlenk technique

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / 1,2-dimethoxyethane; water / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; Iodine monochloride; potassium carbonate; In 1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

2,6-dichloroanisole (1984-65-2) → C26H30Cl2N2O5 (1430799-17-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 3.5 h / -78 - -65 °C / Inert atmosphere; Schlenk technique

1.2: 1 h / -75 - -65 °C / Inert atmosphere; Schlenk technique

2.1: Iodine monochloride / dichloromethane / 20 °C / Cooling with ice

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 24.08 h / 80 °C / Inert atmosphere; Schlenk technique

4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / 1,2-dimethoxyethane; water / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; Iodine monochloride; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

2,4-dichloro-1,5-diiodo-3-methoxybenzene (1221589-80-5) → C26H30Cl2N2O5 (1430799-17-9)

Guidance literature:

Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 24.08 h / 80 °C / Inert atmosphere; Schlenk technique

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / 1,2-dimethoxyethane; water / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; potassium carbonate; In 1,2-dimethoxyethane; water; dimethyl sulfoxide;

upstream raw materials:

C₇H₁₁NO₂

2,2'-(4,6-dichloro-5-methoxy-1,3-phenylene)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

C₇H₁₂INO₂

C₁₂H₁₄INO₂

Downstream raw materials:

C₂₆H₂₈N₂O₅