Technology Process of C17H26Cl2N2O2
There total 8 articles about C17H26Cl2N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
7-<4-phenyl>heptanoic acid;
With
4-methyl-morpholine; chloroformic acid ethyl ester;
In
diethyl ether;
at 0 ℃;
for 0.166667h;
With
hydroxylamine;
In
methanol;
at 20 ℃;
for 0.25h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogen / palladium on activated charcoal / methanol / 4 h / 20 °C / Inert atmosphere
2.1: sodium acetate; acetic acid / water / 10 - 20 °C
3.1: thionyl chloride / chloroform / 5 h / 20 °C / Cooling with ice bath
4.1: 4-methyl-morpholine; chloroformic acid ethyl ester / diethyl ether / 0.17 h / 0 °C
4.2: 0.25 h / 20 °C
With
4-methyl-morpholine; thionyl chloride; hydrogen; sodium acetate; chloroformic acid ethyl ester; acetic acid;
palladium on activated charcoal;
In
methanol; diethyl ether; chloroform; water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0 °C
2.1: water; potassium hydroxide / 1.25 h / Heating; Reflux
3.1: hydrogen / palladium on activated charcoal / methanol / 4 h / 20 °C / Inert atmosphere
4.1: sodium acetate; acetic acid / water / 10 - 20 °C
5.1: thionyl chloride / chloroform / 5 h / 20 °C / Cooling with ice bath
6.1: 4-methyl-morpholine; chloroformic acid ethyl ester / diethyl ether / 0.17 h / 0 °C
6.2: 0.25 h / 20 °C
With
4-methyl-morpholine; thionyl chloride; water; hydrogen; sodium acetate; chloroformic acid ethyl ester; acetic acid; potassium hydroxide; lithium diisopropyl amide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; diethyl ether; chloroform; water;