(E)-2-bromo-3,4,5-trimethoxy-1-styrylbenzene

Base Information

Chemical Name:(E)-2-bromo-3,4,5-trimethoxy-1-styrylbenzene
CAS No.:1310800-01-1
Molecular Formula:C₁₇H₁₇BrO₃
Molecular Weight:349.224
Hs Code.:

Synonyms:(E)-2-bromo-3,4,5-trimethoxy-1-styrylbenzene

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Chemical Property of (E)-2-bromo-3,4,5-trimethoxy-1-styrylbenzene

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Technology Process of (E)-2-bromo-3,4,5-trimethoxy-1-styrylbenzene

There total 1 articles about (E)-2-bromo-3,4,5-trimethoxy-1-styrylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1080-32-6
O,O-diethyl benzylphosphonate

: 35274-53-4
2-bromo-3,4,5-tri-methoxybenzaldehyde

: 1310800-01-1
(E)-2-bromo-3,4,5-trimethoxy-1-styrylbenzene

Guidance literature:: O,O-diethyl benzylphosphonate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

2-bromo-3,4,5-tri-methoxybenzaldehyde; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/jacs.7b01114

Reference yield: 78.0%

: 1310800-01-1
(E)-2-bromo-3,4,5-trimethoxy-1-styrylbenzene

: 60011-16-7
(_S_S)-(+)-tert-butyl tert-butanethiosulfinate

: 1310800-19-1
C₂₁H₂₆O₄S

Guidance literature:: (E)-2-bromo-3,4,5-trimethoxy-1-styrylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

(_S_S)-(+)-tert-butyl tert-butanethiosulfinate; In tetrahydrofuran; hexane; at -78 ℃; for 1h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ol201151r

Reference yield: 42.0%

: 1310800-01-1
(E)-2-bromo-3,4,5-trimethoxy-1-styrylbenzene

: 308103-40-4
(2-acetylphenyl)boronic acid

: (E)-1-(2',3',4'-trimethoxy-6'-styryl-[1,1'-biphenyl]-2-yl)ethan-1-one

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; In water; N,N-dimethyl-formamide; at 150 ℃; for 0.333333h; under 760.051 Torr; Microwave irradiation;
DOI:10.1021/jacs.7b01114