phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside
CAS No.:84333-52-8
Molecular Formula:C₅₇H₆₇NO₂₀
Molecular Weight:1086.15
Hs Code.:

phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

Synonyms:phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

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Chemical Property of phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

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Technology Process of phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

There total 5 articles about phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 33639-77-9
perbenzyl fucosyl bromide

: 84333-51-7
phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 84333-52-8
phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

Guidance literature:: With tetraethylammonium bromide; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; for 120h; Ambient temperature;
DOI:10.1016/0008-6215(83)88287-1

Reference yield:

: 78489-49-3,117436-77-8
phenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-β-D-glucopyranoside

: 84333-52-8
phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / mercuric cyanide / benzene; nitromethane / 52 h / 60 °C

2: 68 percent / 80 percent acetic acid / 0.33 h / 60 °C

3: 67 percent / imidazole / CH₂Cl₂ / 72 h / Heating

4: 73 percent / tetraethylammonium bromide, diisopropylethylamine / CH₂Cl₂; dimethylformamide / 120 h / Ambient temperature

With 1H-imidazole; tetraethylammonium bromide; mercury(II) cyanide; acetic acid; N-ethyl-N,N-diisopropylamine; In nitromethane; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/0008-6215(83)88287-1

Reference yield:

: 84333-50-6
phenyl 2-acetamido-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 84333-52-8
phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / imidazole / CH₂Cl₂ / 72 h / Heating

2: 73 percent / tetraethylammonium bromide, diisopropylethylamine / CH₂Cl₂; dimethylformamide / 120 h / Ambient temperature

With 1H-imidazole; tetraethylammonium bromide; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(83)88287-1