phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside
CAS No.:84333-51-7
Molecular Formula:C₃₀H₃₉NO₁₆
Molecular Weight:669.637
Hs Code.:

Synonyms:phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Chemical Property of phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Technology Process of phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

There total 4 articles about phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 84333-50-6
phenyl 2-acetamido-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 75-36-5
acetyl chloride

: 84333-51-7
phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: With 1H-imidazole; In dichloromethane; for 72h; Heating;
DOI:10.1016/0008-6215(83)88287-1

Reference yield:

: 78489-49-3,117436-77-8
phenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-β-D-glucopyranoside

: 84333-51-7
phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / mercuric cyanide / benzene; nitromethane / 52 h / 60 °C

2: 68 percent / 80 percent acetic acid / 0.33 h / 60 °C

3: 67 percent / imidazole / CH₂Cl₂ / 72 h / Heating

With 1H-imidazole; mercury(II) cyanide; acetic acid; In nitromethane; dichloromethane; benzene;
DOI:10.1016/0008-6215(83)88287-1

Reference yield:

: 76850-48-1,84333-49-3
phenyl 2-acetamido-2-deoxy-4,6-O-(p-methoxybenzylidene)-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 84333-51-7
phenyl 2-acetamido-6-O-acetyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / 80 percent acetic acid / 0.33 h / 60 °C

2: 67 percent / imidazole / CH₂Cl₂ / 72 h / Heating

With 1H-imidazole; acetic acid; In dichloromethane;
DOI:10.1016/0008-6215(83)88287-1