C₆₂H₉₅ClO₁₃SSi₂

Base Information

Chemical Name:C₆₂H₉₅ClO₁₃SSi₂
CAS No.:1053711-39-9
Molecular Formula:C₆₂H₉₅ClO₁₃SSi₂
Molecular Weight:1172.12
Hs Code.:

C<sub>62</sub>H<sub>95</sub>ClO<sub>13</sub>SSi<sub>2</sub>

Synonyms:C₆₂H₉₅ClO₁₃SSi₂

Suppliers and Price of C₆₂H₉₅ClO₁₃SSi₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₂H₉₅ClO₁₃SSi₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₂H₉₅ClO₁₃SSi₂

There total 49 articles about C₆₂H₉₅ClO₁₃SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 4124-41-8
p-toluenesulfonylanhydride

: C₅₅H₈₉ClO₁₁Si₂

: 1053711-39-9
C₆₂H₉₅ClO₁₃SSi₂

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1002/(sici)1521-3773(19980202)37:1/2<190::aid-anie190>3.0.co;2-0

Reference yield:

: 3-Methyl-1-triisopropylsilanyloxy-pent-4-en-2-ol

: 1053711-39-9
C₆₂H₉₅ClO₁₃SSi₂

Guidance literature:: Multi-step reaction with 21 steps

1: 84 percent / NaH, TBAI / tetrahydrofuran / 0 - 20 °C

2: N-methylmorpholine N-oxide, OsO₄, H₂O / tetrahydrofuran

3: aq. NaIO₄ / methanol / 0 - 20 °C

4: toluene / -78 °C

5: 2,6-lutidine / CH₂Cl₂ / 0 - 20 °C

6: Li, NH₃ / tetrahydrofuran / -78 °C

7: Et₃N / diethyl ether

8: hydrogen fluoride pyridine complex, pyridine / tetrahydrofuran

9: 92 percent / KOH / methanol

10: 87 percent / BuLi / -78 - 20 °C

11: 85 percent / Li, NH₃ / tetrahydrofuran / -78 °C

12: N-methylmorpholine N-oxide, OsO₄, H₂O / tetrahydrofuran

13: aq. NaIO₄ / methanol / 0 - 20 °C

14: 1.) diketene acetone adduct, Et₃N / 1.) hexane, 70 deg C, 2.) 125 deg C, 0.2 Torr

15: 1.) tert-BuLi, Bu₃SnCl, 2.) NIS, K₂CO₃ / 1.) THF, -78 to -30 deg C; -78 to 20 deg C, 2.) 0 deg C

16: 1.) tert-BuLi, MgBr₂ / 1.) Et₂O, -78 deg C, 2.) -78 to -50 deg C

17: 1.) NIS, CaCO₃, 2.) Bu₃SnH, AIBN / 1.) MeOH, THF, CH₃CN, 0-20 deg C, 2.) THF, PhBr, 80 deg C

18: 76 percent / TBAF / tetrahydrofuran

19: 75 percent / imidazole / dimethylformamide

20: 78 percent / hydrogen fluoride pyridine complex, pyridine / tetrahydrofuran; methanol

21: 75 percent / (i-Pr)2NEt, DMAP / CH₂Cl₂

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; dmap; potassium hydroxide; sodium periodate; N-iodo-succinimide; osmium(VIII) oxide; n-butyllithium; 2,2'-azobis(isobutyronitrile); diketene acetone; tributyltin chloride; tetrabutyl ammonium fluoride; ammonia; water; tert.-butyl lithium; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; lithium; sodium hydride; potassium carbonate; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; calcium carbonate; magnesium bromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/(sici)1521-3773(19980202)37:1/2<190::aid-anie190>3.0.co;2-0

Reference yield:

: (2-Benzyloxy-3-methyl-pent-4-enyloxy)-triisopropyl-silane

: 1053711-39-9
C₆₂H₉₅ClO₁₃SSi₂

Guidance literature:: Multi-step reaction with 20 steps

1: N-methylmorpholine N-oxide, OsO₄, H₂O / tetrahydrofuran

2: aq. NaIO₄ / methanol / 0 - 20 °C

3: toluene / -78 °C

4: 2,6-lutidine / CH₂Cl₂ / 0 - 20 °C

5: Li, NH₃ / tetrahydrofuran / -78 °C

6: Et₃N / diethyl ether

7: hydrogen fluoride pyridine complex, pyridine / tetrahydrofuran

8: 92 percent / KOH / methanol

9: 87 percent / BuLi / -78 - 20 °C

10: 85 percent / Li, NH₃ / tetrahydrofuran / -78 °C

11: N-methylmorpholine N-oxide, OsO₄, H₂O / tetrahydrofuran

12: aq. NaIO₄ / methanol / 0 - 20 °C

13: 1.) diketene acetone adduct, Et₃N / 1.) hexane, 70 deg C, 2.) 125 deg C, 0.2 Torr

14: 1.) tert-BuLi, Bu₃SnCl, 2.) NIS, K₂CO₃ / 1.) THF, -78 to -30 deg C; -78 to 20 deg C, 2.) 0 deg C

15: 1.) tert-BuLi, MgBr₂ / 1.) Et₂O, -78 deg C, 2.) -78 to -50 deg C

16: 1.) NIS, CaCO₃, 2.) Bu₃SnH, AIBN / 1.) MeOH, THF, CH₃CN, 0-20 deg C, 2.) THF, PhBr, 80 deg C

17: 76 percent / TBAF / tetrahydrofuran

18: 75 percent / imidazole / dimethylformamide

19: 78 percent / hydrogen fluoride pyridine complex, pyridine / tetrahydrofuran; methanol

20: 75 percent / (i-Pr)2NEt, DMAP / CH₂Cl₂

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; dmap; potassium hydroxide; sodium periodate; N-iodo-succinimide; osmium(VIII) oxide; n-butyllithium; 2,2'-azobis(isobutyronitrile); diketene acetone; tributyltin chloride; tetrabutyl ammonium fluoride; ammonia; water; tert.-butyl lithium; tri-n-butyl-tin hydride; lithium; potassium carbonate; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; calcium carbonate; magnesium bromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/(sici)1521-3773(19980202)37:1/2<190::aid-anie190>3.0.co;2-0