1(R)-(dimethoxymethyl)-2(S)-(phenylthio)-3(S)-methyl-4(S)-<(2,4-dinitrophenyl)amino>-8-methoxy-1,2,3,4-tetrahydronaphthalene

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Chemical Name:1(R*)-(dimethoxymethyl)-2(S*)-(phenylthio)-3(S*)-methyl-4(S*)-<(2,4-dinitrophenyl)amino>-8-methoxy-1,2,3,4-tetrahydronaphthalene
CAS No.:118629-83-7
Molecular Formula:C₂₇H₂₉N₃O₇S
Molecular Weight:539.609
Hs Code.:

Synonyms:1(R*)-(dimethoxymethyl)-2(S*)-(phenylthio)-3(S*)-methyl-4(S*)-<(2,4-dinitrophenyl)amino>-8-methoxy-1,2,3,4-tetrahydronaphthalene

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Chemical Property of 1(R*)-(dimethoxymethyl)-2(S*)-(phenylthio)-3(S*)-methyl-4(S*)-<(2,4-dinitrophenyl)amino>-8-methoxy-1,2,3,4-tetrahydronaphthalene

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Technology Process of 1(R*)-(dimethoxymethyl)-2(S*)-(phenylthio)-3(S*)-methyl-4(S*)-<(2,4-dinitrophenyl)amino>-8-methoxy-1,2,3,4-tetrahydronaphthalene

There total 3 articles about 1(R*)-(dimethoxymethyl)-2(S*)-(phenylthio)-3(S*)-methyl-4(S*)-<(2,4-dinitrophenyl)amino>-8-methoxy-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: (1S,8R,10R,11S,12S)-9-(2,4-Dinitro-phenyl)-3,10-dimethoxy-12-methyl-11-phenylsulfanyl-9-aza-tricyclo[6.2.2.0^2,7]dodeca-2,4,6-triene

: 118629-83-7
1(R*)-(dimethoxymethyl)-2(S*)-(phenylthio)-3(S*)-methyl-4(S*)-<(2,4-dinitrophenyl)amino>-8-methoxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With Dowex-50x8-400; In methanol; for 24h; Ambient temperature;
DOI:10.1021/jo00266a019

Reference yield:

: 22103-05-5
phenyl (Z)-(1-propenyl) sulfide

: 118629-83-7
1(R*)-(dimethoxymethyl)-2(S*)-(phenylthio)-3(S*)-methyl-4(S*)-<(2,4-dinitrophenyl)amino>-8-methoxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: CaCO₃ / methanol / 72 h / 25 - 40 °C

2: 72 percent / Dowex-50X₈-400 / methanol / 24 h / Ambient temperature

With Dowex-50x8-400; calcium carbonate; In methanol;
DOI:10.1021/jo00266a019

Reference yield:

: 2-(2,4-Dinitro-phenyl)-5-methoxy-isoquinolinium

: 118629-83-7
1(R*)-(dimethoxymethyl)-2(S*)-(phenylthio)-3(S*)-methyl-4(S*)-<(2,4-dinitrophenyl)amino>-8-methoxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: CaCO₃ / methanol / 72 h / 25 - 40 °C

2: 72 percent / Dowex-50X₈-400 / methanol / 24 h / Ambient temperature

With Dowex-50x8-400; calcium carbonate; In methanol;
DOI:10.1021/jo00266a019