1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluorohexadec-7-ene

Base Information

Chemical Name:1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluorohexadec-7-ene
CAS No.:120464-27-9
Molecular Formula:C16H19 F13
Molecular Weight:458.306
Hs Code.:2903590090
DSSTox Substance ID:DTXSID10379855
Mol file:120464-27-9.mol

Synonyms:1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorohexadec-7-ene;120464-27-9;SCHEMBL9226908;DTXSID10379855;UFXJXRIUXCGTRG-UHFFFAOYSA-N;FT-0765811

Suppliers and Price of 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluorohexadec-7-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
1-(Perfluorohexyl)dec-1-ene
25 g
$ 327.00

American Custom Chemicals Corporation
1-(PERFLUOROHEXYL)DEC-1-ENE 95.00%
5G
$ 924.12

Total 8 raw suppliers

Chemical Property of 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluorohexadec-7-ene

Chemical Property:

Boiling Point:276.6±8.0 °C(Predicted)
PSA：0.00000
Density:1.282±0.06 g/cm3(Predicted)
LogP:8.03200
XLogP3:9.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:13
Rotatable Bond Count:12
Exact Mass:458.1279167
Heavy Atom Count:29
Complexity:531

Purity/Quality:

99%, ^*data from raw suppliers

1-(Perfluorohexyl)dec-1-ene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCC=CC(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F

Technology Process of 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluorohexadec-7-ene

There total 4 articles about 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluorohexadec-7-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 764-93-2
1-decyne

: 355-43-1
n-perfluorohexyl iodide

: 307-24-4
undecafluorohexanoic acid

: 120464-27-9
1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorohexadec-7-ene

Guidance literature:: With disodium hydrogenphosphate; potassium dihydrogenphosphate; urease; at 25 - 30 ℃;
DOI:10.1021/jo00245a041

Reference yield:

: 764-93-2
1-decyne

: 335-56-8
1-bromo-1,1,2,2,3,3,4,4,5,5,6,6,6-tridecafluorohexane

: 120464-27-9
1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorohexadec-7-ene

: 1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorohexadec-7-ene

Guidance literature:: With Eosin Y; water; sodium thiosulfate; In tetrahydrofuran; acetonitrile; at 20 ℃; for 17h; Overall yield = 35%; Overall yield = 32.1 mg; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.8b03596

Reference yield:

: 764-93-2
1-decyne

: 355-41-9
perfluoro-n-hexyl chloride

: 120464-27-9
1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorohexadec-7-ene

: 1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorohexadec-7-ene

Guidance literature:: With triphenylphosphine; nickel dichloride; zinc; In N,N-dimethyl-formamide; at 100 ℃; for 7h; Title compound not separated from byproducts.;
DOI:10.1021/jo010178j