Technology Process of Aceteic acid, methoxy-, 3-methyl-2-(phenylmethoxy)-1-(1-propenyl)-4-undecenyl ester, (1R*(E),2R*,3R*,4E)-
There total 7 articles about Aceteic acid, methoxy-, 3-methyl-2-(phenylmethoxy)-1-(1-propenyl)-4-undecenyl ester, (1R*(E),2R*,3R*,4E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
DOI:10.1021/jo00226a032
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 95 percent / pyridine / tetrahydrofuran / 2 h / 0 °C
2: 1.) LDA / 1.) THF, -78 deg C, 1.5 min, 2.) THF, -78 deg C, 10 min
3: tetrahydrofuran / 2 h / -78 - 25 °C
4: LiAlH4 / tetrahydrofuran / 0 °C
5: 99 percent / (COCl)2, (CH3)2SO, (C2H5)3N / CH2Cl2 / 1 h / Ambient temperature
6: 72 percent / MgBr2*Et2O / diethyl ether; benzene / 0.5 h / -78 - 25 °C
7: 91 percent / pyridine / tetrahydrofuran / 1 h / 0 °C
With
pyridine; lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; magnesium bromide; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; dichloromethane; benzene;
DOI:10.1021/jo00226a032
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / (COCl)2, (CH3)2SO, (C2H5)3N / CH2Cl2 / 1 h / Ambient temperature
2: 72 percent / MgBr2*Et2O / diethyl ether; benzene / 0.5 h / -78 - 25 °C
3: 91 percent / pyridine / tetrahydrofuran / 1 h / 0 °C
With
pyridine; oxalyl dichloride; dimethyl sulfoxide; triethylamine; magnesium bromide;
In
tetrahydrofuran; diethyl ether; dichloromethane; benzene;
DOI:10.1021/jo00226a032
