1-(4-{10-[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetraphenylcyclooctadeca-1,2,3,7,8,9,13,14,15-nonaen-5,11,17-triyn-1-yl}phenyl)-1H-indole (p-bis(4-(indol-1-yl)phenyl)-tetra-phenyl-carbobenzene)

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Chemical Name:1-(4-{10-[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetraphenylcyclooctadeca-1,2,3,7,8,9,13,14,15-nonaen-5,11,17-triyn-1-yl}phenyl)-1H-indole (p-bis(4-(indol-1-yl)phenyl)-tetra-phenyl-carbobenzene)
CAS No.:1394958-91-8
Molecular Formula:C₇₀H₄₀N₂
Molecular Weight:909.101
Hs Code.:

1-(4-{10-[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetraphenylcyclooctadeca-1,2,3,7,8,9,13,14,15-nonaen-5,11,17-triyn-1-yl}phenyl)-1H-indole (p-bis(4-(indol-1-yl)phenyl)-tetra-phenyl-carbobenzene)

Synonyms:1-(4-{10-[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetraphenylcyclooctadeca-1,2,3,7,8,9,13,14,15-nonaen-5,11,17-triyn-1-yl}phenyl)-1H-indole (p-bis(4-(indol-1-yl)phenyl)-tetra-phenyl-carbobenzene)

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Chemical Property of 1-(4-{10-[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetraphenylcyclooctadeca-1,2,3,7,8,9,13,14,15-nonaen-5,11,17-triyn-1-yl}phenyl)-1H-indole (p-bis(4-(indol-1-yl)phenyl)-tetra-phenyl-carbobenzene)

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Technology Process of 1-(4-{10-[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetraphenylcyclooctadeca-1,2,3,7,8,9,13,14,15-nonaen-5,11,17-triyn-1-yl}phenyl)-1H-indole (p-bis(4-(indol-1-yl)phenyl)-tetra-phenyl-carbobenzene)

There total 2 articles about 1-(4-{10-[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetraphenylcyclooctadeca-1,2,3,7,8,9,13,14,15-nonaen-5,11,17-triyn-1-yl}phenyl)-1H-indole (p-bis(4-(indol-1-yl)phenyl)-tetra-phenyl-carbobenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1394958-90-7
1,10-bis[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetramethoxy-4,7,13,16-tetraphenylcyclooctadeca-2,5,8,11,14,17-hexayne-1,10-diol

: 1394958-91-8
1-(4-{10-[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetraphenylcyclooctadeca-1,2,3,7,8,9,13,14,15-nonaen-5,11,17-triyn-1-yl}phenyl)-1H-indole (p-bis(4-(indol-1-yl)phenyl)-tetra-phenyl-carbobenzene)

Guidance literature:: 1,10-bis[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetramethoxy-4,7,13,16-tetraphenylcyclooctadeca-2,5,8,11,14,17-hexayne-1,10-diol; With hydrogenchloride; tin(ll) chloride; In diethyl ether; dichloromethane; at -78 - -10 ℃; for 3h; Inert atmosphere;

With sodium hydroxide; In diethyl ether; dichloromethane; water; at -10 - 20 ℃; Inert atmosphere;
DOI:10.1039/c2cc34176j

Reference yield:

: 4,7,13,16-tetramethoxy-4,7,13,16-tetraphenylcyclooctadeca-2,5,8,11,14,17-hexayne-1,10-dione

: 174621-52-4
N-(4-bromophenyl)-1H-indole

: 1394958-91-8
1-(4-{10-[4-(1H-indol-1-yl)phenyl]-4,7,13,16-tetraphenylcyclooctadeca-1,2,3,7,8,9,13,14,15-nonaen-5,11,17-triyn-1-yl}phenyl)-1H-indole (p-bis(4-(indol-1-yl)phenyl)-tetra-phenyl-carbobenzene)

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / tetrahydrofuran / 20 °C / Inert atmosphere

1.2: 18 h / 0 - 20 °C / Inert atmosphere

2.1: hydrogenchloride; tin(ll) chloride / diethyl ether; dichloromethane / 3 h / -78 - -10 °C / Inert atmosphere

2.2: -10 - 20 °C / Inert atmosphere

With hydrogenchloride; magnesium; tin(ll) chloride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1039/c2cc34176j