C₂₆H₂₇NO₂Si

Base Information

Chemical Name:C₂₆H₂₇NO₂Si
CAS No.:1360144-80-4
Molecular Formula:C₂₆H₂₇NO₂Si
Molecular Weight:413.591
Hs Code.:

C<sub>26</sub>H<sub>27</sub>NO<sub>2</sub>Si

Synonyms:C₂₆H₂₇NO₂Si

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Chemical Property of C₂₆H₂₇NO₂Si

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Technology Process of C₂₆H₂₇NO₂Si

There total 7 articles about C₂₆H₂₇NO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 136918-14-4,85-41-6
phthalimide

: 1360144-87-1
2-(2-(trimethylsilylmethyl)benzyl)benzyl alcohol

: 1360144-80-4
C₂₆H₂₇NO₂Si

Guidance literature:: With di-isopropyl azodicarboxylate; In tetrahydrofuran; at 20 ℃; for 15h;
DOI:10.1007/s11164-011-0422-8

Reference yield:

: 17100-66-2
2-(tetrahydropyranyloxy)methylbromobenzene

: 1360144-80-4
C₂₆H₂₇NO₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

1.2: 1 h / -78 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene / 4 h / 80 °C

3.1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

4.1: di-isopropyl azodicarboxylate / tetrahydrofuran / 15 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; di-isopropyl azodicarboxylate; sodium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; water; toluene; 4.1: Mitsunobu reaction;
DOI:10.1007/s11164-011-0422-8

Reference yield:

: 89-95-2
2-methyl-benzyl alcohol

: 1360144-80-4
C₂₆H₂₇NO₂Si

Guidance literature:: Multi-step reaction with 5 steps

1: n-butyllithium

2: carbon tetrabromide; triphenylphosphine / diethyl ether / 24 h / 0 - 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene / 4 h / 80 °C

4: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

5: di-isopropyl azodicarboxylate / tetrahydrofuran / 15 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; carbon tetrabromide; di-isopropyl azodicarboxylate; sodium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; water; toluene; 5: Mitsunobu reaction;
DOI:10.1007/s11164-011-0422-8