C₆₀H₆₃Cl₂N₅O₁₁Si

Base Information

Chemical Name:C₆₀H₆₃Cl₂N₅O₁₁Si
CAS No.:1438408-36-6
Molecular Formula:C₆₀H₆₃Cl₂N₅O₁₁Si
Molecular Weight:1129.18
Hs Code.:

C<sub>60</sub>H<sub>63</sub>Cl<sub>2</sub>N<sub>5</sub>O<sub>11</sub>Si

Synonyms:C₆₀H₆₃Cl₂N₅O₁₁Si

Suppliers and Price of C₆₀H₆₃Cl₂N₅O₁₁Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₀H₆₃Cl₂N₅O₁₁Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₀H₆₃Cl₂N₅O₁₁Si

There total 14 articles about C₆₀H₆₃Cl₂N₅O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1438408-35-5
C₅₄H₄₉Cl₂N₅O₁₁

: 69739-34-0
t-butyldimethylsiyl triflate

: 1438408-36-6
C₆₀H₆₃Cl₂N₅O₁₁Si

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at -78 ℃; for 6h; Cooling with ice; Inert atmosphere;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-16-2
C₁₄H₂₅NO₄

: 1438408-36-6
C₆₀H₆₃Cl₂N₅O₁₁Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / Cooling with ice; Inert atmosphere

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere

2.2: 8 h / 20 °C / Inert atmosphere

2.3: 3.33 h / 20 °C / Inert atmosphere

3.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

5.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

6.2: 0.5 h / -78 °C / Inert atmosphere

7.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10.33 h / -40 - -20 °C / Inert atmosphere

9.1: Trimethyl borate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere

9.2: 3 h / 50 °C / Inert atmosphere

10.1: hydrogenchloride / methanol; water / 10 h / 40 °C / Inert atmosphere

11.1: N-ethyl-N,N-diisopropylamine / 0 °C / Inert atmosphere

11.2: 0 - 20 °C / Inert atmosphere

12.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

13.1: 2,6-dimethylpyridine / dichloromethane / 6 h / -78 °C / Cooling with ice; Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; hydrogenchloride; Trimethyl borate; C₁₅H₂₆Cl₂CuN₂O₂; iodine; mercuric triflate; diisobutylaluminium hydride; sodium hydrogencarbonate; caesium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 4.1: |Dess-Martin Oxidation / 5.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-19-5
C₂₅H₃₈N₂O₇

: 1438408-36-6
C₆₀H₆₃Cl₂N₅O₁₁Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

3.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

4.2: 0.5 h / -78 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10.33 h / -40 - -20 °C / Inert atmosphere

7.1: Trimethyl borate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere

7.2: 3 h / 50 °C / Inert atmosphere

8.1: hydrogenchloride / methanol; water / 10 h / 40 °C / Inert atmosphere

9.1: N-ethyl-N,N-diisopropylamine / 0 °C / Inert atmosphere

9.2: 0 - 20 °C / Inert atmosphere

10.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

11.1: 2,6-dimethylpyridine / dichloromethane / 6 h / -78 °C / Cooling with ice; Inert atmosphere

With 2,6-dimethylpyridine; hydrogenchloride; Trimethyl borate; C₁₅H₂₆Cl₂CuN₂O₂; mercuric triflate; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 2.1: |Dess-Martin Oxidation / 3.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d