Fe3(CO)9(μ3-η2-Et2N2)

Base Information

Chemical Name:Fe3(CO)9(μ3-η2-Et2N2)
CAS No.:107556-56-9
Molecular Formula:C₁₃H₁₀Fe₃N₂O₉
Molecular Weight:505.771
Hs Code.:

Synonyms:Fe3(CO)9(μ3-η2-Et2N2)

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Chemical Property of Fe3(CO)9(μ3-η2-Et2N2)

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Technology Process of Fe3(CO)9(μ3-η2-Et2N2)

There total 1 articles about Fe3(CO)9(μ3-η2-Et2N2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 133551-93-6
(Fe(CO)3)3(NC₂H₅)2CHCC₆H₅

: 107556-56-9
Fe3(CO)9(μ3-η2-Et2N2)

: 118682-17-0
Fe(CO)3N(C₂H₅)N(C₂H₅)FeC₄H₂(C₆H₅)2(CO)Fe(CO)3

: 118682-16-9
Fe(CO)3N(C₂H₅)N(C₂H₅)FeC₄H₂(C₆H₅)2(CO)Fe(CO)3

: 56924-78-8
Fe2(CO)6(μN2Et2)

Guidance literature:: In n-heptane; under CO, stirred vigorously at 80°C for 20 min; volume reduced to dryness, thin-layer-chromatography;

Reference yield: 79.0%

: 107556-56-9
Fe3(CO)9(μ3-η2-Et2N2)

: 425-75-2
trifluoromethanesulfonic acid ethyl ester

: 591-51-5
phenyllithium

: 56924-78-8
Fe2(CO)6(μN2Et2)

: 133551-90-3
Fe(CO)3Fe(CO)3Fe(CO)2COC₂H₅C₆H₅(C₂H₅NNC₂H₅)

Guidance literature:: In diethyl ether; PhLi added dropwise at 0°C for 20 min, EtOTf added, stirred 1 h at 0°C, stirred 4 h at room temperature; solvent removed in vacuo, chromatographed with hexane/CH2Cl2, elem. anal.;

Reference yield: 61.0%

: 107556-56-9
Fe3(CO)9(μ3-η2-Et2N2)

: 536-74-3
phenylacetylene

: 133551-93-6
(Fe(CO)3)3(NC₂H₅)2CHCC₆H₅

Guidance literature:: With Me₃NO; In dichloromethane; under CO, organic compounds added over 1 h dropwise under vigorously stirring; volume reduced in vacuo to dryness, extracted with hexane, chromatographed (silica gel, hexane/CH2Cl2), elem. anal.;