Fe2(CO)6(μN2Et2)

Base Information

Chemical Name:Fe2(CO)6(μN2Et2)
CAS No.:56924-78-8
Molecular Formula:C₁₀H₁₀Fe₂N₂O₆
Molecular Weight:365.893
Hs Code.:

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Chemical Property of Fe2(CO)6(μN2Et2)

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Technology Process of Fe2(CO)6(μN2Et2)

There total 3 articles about Fe2(CO)6(μN2Et2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 133551-93-6
(Fe(CO)3)3(NC₂H₅)2CHCC₆H₅

: 107556-56-9
Fe3(CO)9(μ3-η2-Et2N2)

: 118682-17-0
Fe(CO)3N(C₂H₅)N(C₂H₅)FeC₄H₂(C₆H₅)2(CO)Fe(CO)3

: 118682-16-9
Fe(CO)3N(C₂H₅)N(C₂H₅)FeC₄H₂(C₆H₅)2(CO)Fe(CO)3

: 56924-78-8
Fe2(CO)6(μN2Et2)

Guidance literature:: In n-heptane; under CO, stirred vigorously at 80°C for 20 min; volume reduced to dryness, thin-layer-chromatography;

Reference yield: 79.0%

: 107556-56-9
Fe3(CO)9(μ3-η2-Et2N2)

: 425-75-2
trifluoromethanesulfonic acid ethyl ester

: 591-51-5
phenyllithium

: 56924-78-8
Fe2(CO)6(μN2Et2)

: 133551-90-3
Fe(CO)3Fe(CO)3Fe(CO)2COC₂H₅C₆H₅(C₂H₅NNC₂H₅)

Guidance literature:: In diethyl ether; PhLi added dropwise at 0°C for 20 min, EtOTf added, stirred 1 h at 0°C, stirred 4 h at room temperature; solvent removed in vacuo, chromatographed with hexane/CH2Cl2, elem. anal.;