2-(2,3,4,5,6-pentafluoroanilino)tropone

Base Information

Chemical Name:2-(2,3,4,5,6-pentafluoroanilino)tropone
CAS No.:259266-43-8
Molecular Formula:C₁₃H₆F₅NO
Molecular Weight:287.189
Hs Code.:

Synonyms:2-(2,3,4,5,6-pentafluoroanilino)tropone

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Chemical Property of 2-(2,3,4,5,6-pentafluoroanilino)tropone

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Technology Process of 2-(2,3,4,5,6-pentafluoroanilino)tropone

There total 2 articles about 2-(2,3,4,5,6-pentafluoroanilino)tropone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 771-60-8
2,3,4,5,6-pentafluoroaniline

: 112533-23-0
2-(trifluoromethylsulfonylhydroxy)cyclohepta-2,4,6-triene-1-one

: 259266-43-8
2-(2,3,4,5,6-pentafluoroanilino)tropone

Guidance literature:: With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 80 ℃; for 15.5h;
DOI:10.1021/ol991310t

Reference yield: 84.0%

: 259266-43-8
2-(2,3,4,5,6-pentafluoroanilino)tropone

Guidance literature:

Reference yield: 87.0%

: 1270-98-0
cyclopentadienyl titanium(IV) trichloride

: 7732-18-5
water

: 259266-43-8
2-(2,3,4,5,6-pentafluoroanilino)tropone

: 868134-87-6
dichloromonocyclopentadienyl[2-(2,3,4,5,6-pentafluoroanilino)tropone]titanium(IV)

: (cyclopentadienyl)[2-(2,3,4,5,6-pentafluoroanilino)tropone]TiCl-O-TiCl₂(cyclopentadienyl)*(dichloromethane)

Guidance literature:: With n-BuLi; In tetrahydrofuran; under N2; n-BuLi added dropwise at -78°C to ligand in THF; stirred at -78°C for 1 h, then at room temp.; added dropwise to soln. of Ti complex in THF at -78°C; warmed slowly to ambient temp.; stirred for 1 h; solvent removed in vac.; dissolved in min. CH2Cl2; soln. filtered through Celite; layered with hexane; single crystals of Ti-Cl2 complex obtained; single crystals of Ti-Cl complex isolated as byproduct from CH2Cl2-pentane soln.; elem. anal.;
DOI:10.1039/b506079f