methyl 6-hydroxydodecanoate

Base Information

Chemical Name:methyl 6-hydroxydodecanoate
CAS No.:84770-43-4
Molecular Formula:C₁₃H₂₆O₃
Molecular Weight:230.348
Hs Code.:

Synonyms:methyl 6-hydroxydodecanoate

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Chemical Property of methyl 6-hydroxydodecanoate

Chemical Property:

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Technology Process of methyl 6-hydroxydodecanoate

There total 1 articles about methyl 6-hydroxydodecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 143-07-7
lauric acid

: 17287-03-5
trimethylsulphonium hydroxide

: 57084-18-1,2305-05-7
gamma-dodecalactone

: 7370-36-7
5-nonyldihydrofuran-2(3H)-one

: 42550-37-8
5-Hydroxy-laurinsaeuremethylester

: 27512-78-3
methyl 10-hydroxydodecanoate

: 132214-85-8
Methyl (+/-)-γ-hydroxy-γ-octylbutyrate

: 87442-15-7
9-Hydroxy-dodecanoic acid methyl ester

: 109718-22-1
(-)-(R)-11-Hydroxydodecansaeure-methylester

: 84770-43-4
methyl 6-hydroxydodecanoate

Guidance literature:: With glucose dehydrogenase from Bacillus megaterium; cytochrome P₄₅₀ monooxygenase CYP₅₀₅E₃ from Aspergillus terreus; nicotinamide adenine dinucleotide; In aq. phosphate buffer; dimethyl sulfoxide; at 25 ℃; for 24h; regioselective reaction; Enzymatic reaction;
DOI:10.1002/anie.202001055

Reference yield:

: 2628-17-3,24979-70-2
4-Vinylphenol

: 84770-43-4
methyl 6-hydroxydodecanoate

: 328935-19-9
methyl 6-(4-vinylphenoxy)dodecanoate

Guidance literature:: With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In toluene; at -18 - 0 ℃; for 25h;
DOI:10.1021/ja002462i

Reference yield:

: 84770-43-4
methyl 6-hydroxydodecanoate

: 6-(4-vinylphenoxy)dodecanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: tributylphosphine; 1,1'-(azodicarbonyl)dipiperidine / toluene / 25 h / -18 - 0 °C

2: NaOH / methanol; H₂O / 4.5 h / Heating

With sodium hydroxide; tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In methanol; water; toluene;
DOI:10.1021/ja002462i