[2'-O-acetyl-3'-O-(3,4-di-O-acetyl-2,6-di-O-benzyl-α-D-glucopyranosyl)-5'-O-benzyl-β-D-ribofuranosyloxy]prop-3-yne

Base Information

Chemical Name:[2'-O-acetyl-3'-O-(3,4-di-O-acetyl-2,6-di-O-benzyl-α-D-glucopyranosyl)-5'-O-benzyl-β-D-ribofuranosyloxy]prop-3-yne
CAS No.:197644-84-1
Molecular Formula:C₄₁H₄₆O₁₃
Molecular Weight:746.808
Hs Code.:

Synonyms:[2'-O-acetyl-3'-O-(3,4-di-O-acetyl-2,6-di-O-benzyl-α-D-glucopyranosyl)-5'-O-benzyl-β-D-ribofuranosyloxy]prop-3-yne

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2'-O-acetyl-3'-O-(3,4-di-O-acetyl-2,6-di-O-benzyl-α-D-glucopyranosyl)-5'-O-benzyl-β-D-ribofuranosyloxy]prop-3-yne

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Technology Process of [2'-O-acetyl-3'-O-(3,4-di-O-acetyl-2,6-di-O-benzyl-α-D-glucopyranosyl)-5'-O-benzyl-β-D-ribofuranosyloxy]prop-3-yne

There total 2 articles about [2'-O-acetyl-3'-O-(3,4-di-O-acetyl-2,6-di-O-benzyl-α-D-glucopyranosyl)-5'-O-benzyl-β-D-ribofuranosyloxy]prop-3-yne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 107-19-7
propargyl alcohol

: 197644-83-0
1,2-di-O-acetyl-3-O-(3',4'-di-O-acetyl-2',6'-di-O-benzyl-α-D-glucopyranosyl)-5-O-benzyl-α/β-D-ribofuranoside

: 197644-84-1
[2'-O-acetyl-3'-O-(3,4-di-O-acetyl-2,6-di-O-benzyl-α-D-glucopyranosyl)-5'-O-benzyl-β-D-ribofuranosyloxy]prop-3-yne

: 1,2-di-O-acetyl-3-O-(3',4'-di-O-acetyl-2',6'-di-O-benzyl-α-D-glucopyranosyl)-5-O-benzyl-α-D-ribofuranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/jm000957c

Reference yield: 81.0%

: 107-19-7
propargyl alcohol

: 197644-83-0
1,2-di-O-acetyl-3-O-(3',4'-di-O-acetyl-2',6'-di-O-benzyl-α-D-glucopyranosyl)-5-O-benzyl-α/β-D-ribofuranoside

: 197644-84-1
[2'-O-acetyl-3'-O-(3,4-di-O-acetyl-2,6-di-O-benzyl-α-D-glucopyranosyl)-5'-O-benzyl-β-D-ribofuranosyloxy]prop-3-yne

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; for 0.5h;
DOI:10.1016/S0040-4039(97)01811-X

Reference yield: 100.0%

: 624-38-4,1032416-46-8
para-diiodobenzene

: 197644-84-1
[2'-O-acetyl-3'-O-(3,4-di-O-acetyl-2,6-di-O-benzyl-α-D-glucopyranosyl)-5'-O-benzyl-β-D-ribofuranosyloxy]prop-3-yne

: 1,4-bis{[2'-O-acetyl-5'-O-benzyl-3'-O-(3,4-di-O-acetyl-2,6-di-O-benzyl-α-D-glucopyranosyl)-β-D-ribofuranosyloxy]prop-3-ynyl}benzene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; for 2h;
DOI:10.1021/jm000957c