C₃₀H₄₂B₂N₂O₄

Base Information

• Chemical Name: C₃₀H₄₂B₂N₂O₄
• CAS No.: 1174902-09-0
• Molecular Formula: C₃₀H₄₂B₂N₂O₄
• Molecular Weight: 516.296
• Mol file: 1174902-09-0.mol

Synonyms:C₃₀H₄₂B₂N₂O₄

Chemical Property of C₃₀H₄₂B₂N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₄₂B₂N₂O₄

There total 2 articles about C₃₀H₄₂B₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

5-mesityldipyrromethane + bis(pinacol)diborane (73183-34-3) → C30H42B2N2O4 (1174902-09-0)

Guidance literature:

With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine; In 1,4-dioxane; for 48h; Inert atmosphere; Reflux;

DOI:10.1021/acs.orglett.7b00988

Reference yield: 80.0%

5-(mesityl)dipyrromethane (159152-14-4) + bis(pinacol)diborane (73183-34-3) → C24H31BN2O2 (1174902-10-3) + C30H42B2N2O4 (1174902-09-0)

Guidance literature:

With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine; In 1,4-dioxane; at 100 - 105 ℃; for 24h; regioselective reaction; Inert atmosphere;

DOI:10.1002/chem.200802541

Reference yield: 50.0%

C30H42B2N2O4 (1174902-09-0) + 1,2-bis(4-bromophenyl)diazene (1601-98-5) → C42H34Br2N6

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; triphenylphosphine; cesium fluoride; In N,N-dimethyl-formamide; toluene; for 48h; Inert atmosphere; Reflux;

DOI:10.1021/acs.orglett.7b00988

upstream raw materials:

5-(mesityl)dipyrromethane

bis(pinacol)diborane

Downstream raw materials:

C₃₆H₄₈N₂O₄

C₃₆H₄₈N₂O₄