7-benzyloxy-4',5-dihydroxy-3',6,8-trimethoxyflavone 4'-tetra-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:7-benzyloxy-4',5-dihydroxy-3',6,8-trimethoxyflavone 4'-tetra-O-acetyl-β-D-glucopyranoside
CAS No.:83906-33-6
Molecular Formula:C₃₉H₄₀O₁₇
Molecular Weight:780.736
Hs Code.:

Synonyms:7-benzyloxy-4',5-dihydroxy-3',6,8-trimethoxyflavone 4'-tetra-O-acetyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-benzyloxy-4',5-dihydroxy-3',6,8-trimethoxyflavone 4'-tetra-O-acetyl-β-D-glucopyranoside

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Technology Process of 7-benzyloxy-4',5-dihydroxy-3',6,8-trimethoxyflavone 4'-tetra-O-acetyl-β-D-glucopyranoside

There total 4 articles about 7-benzyloxy-4',5-dihydroxy-3',6,8-trimethoxyflavone 4'-tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 70575-19-8
sudachitin 7-benzyl ether

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 83906-33-6
7-benzyloxy-4',5-dihydroxy-3',6,8-trimethoxyflavone 4'-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; acetone; for 168h;
DOI:10.1246/bcsj.55.2928

Reference yield:

: 4281-28-1
sudachitin

: 83906-33-6
7-benzyloxy-4',5-dihydroxy-3',6,8-trimethoxyflavone 4'-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / KI, 1 percent aq. KOH / acetone; dimethylformamide / 96 h / Ambient temperature

2: 44 percent / 2percent aq. KOH / acetone; dimethylformamide / 168 h

With potassium hydroxide; potassium iodide; In N,N-dimethyl-formamide; acetone;
DOI:10.1246/bcsj.55.2928

Reference yield:

: 100-44-7
benzyl chloride

: 83906-33-6
7-benzyloxy-4',5-dihydroxy-3',6,8-trimethoxyflavone 4'-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / KI, 1 percent aq. KOH / acetone; dimethylformamide / 96 h / Ambient temperature

2: 44 percent / 2percent aq. KOH / acetone; dimethylformamide / 168 h

With potassium hydroxide; potassium iodide; In N,N-dimethyl-formamide; acetone;
DOI:10.1246/bcsj.55.2928